Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometer (VSM). The resulting nanocom...

BACKGROUND Lung ultrasound (LUS) can diagnose extravacular lung water (EVLW) through the visualization of B lines in both humans and large animals. However, there are no published data on the use of ultrasound to detect EVLW in rats, the gold standard to evaluate of EVLW in rats is post-mortem gravimetric analysis. The present study was designed to determine the similarity between lung sonograp...

Fecal lipid content is usually determined by titrimetric or gravimetric methods, but these methods are time consuming and involve dangerous solvents. We have developed a new method of measuring fecal lipids by Fourier transform infrared spectrometry (FTIR) with an attenuated total reflectance accessory that is fast and requires no solvents. The spectra of stools from 4000 to 750 cm-1 were analy...

Penetration of liquid pesticides through textile materials is a criterion for determining the performance of protective clothing used by pesticide handlers. The pipette method is frequently used to apply liquid pesticides onto textile materials to measure penetration. Typically, analytical techniques such as Gas Chromatography (GC) are used to measure percentage penetration. These techniques ar...

One of the most important design and operating parameters at composting facilities is moisture content. Existing standard gravimetric oven methods required a minimum of 19 hours to complete. In this study, by reducing the amount of sample, the time required to complete a standard gravimetric oven method was reduced to nine hours. A new infrared moisture balance method was also developed that re...

The molecular building block approach was employed effectively to construct a series of novel isoreticular, highly porous and stable, aluminum-based metal-organic frameworks with soc topology. From this platform, three compounds were experimentally isolated and fully characterized: namely, the parent Al-soc-MOF-1 and its naphthalene and anthracene analogues. Al-soc-MOF-1 exhibits outstanding gr...

A regiospecific bis-adduct of C70 with anthracene was prepared with unusually high yield (68%) by the Diels-Alder reaction in the absence of solvent (melt). The structure of the bis-adduct was an unexpected 12 o'clock isomer, as determined by single crystal X-ray diffraction, thermal gravimetric analysis (TGA) and spectroscopy.

In the estimation of very small q-qantities of material there is no question that colorimetric is preferable to gravimetric analysis. The colorimetric method is generally quicker and simpler to carry out-an important factor when numerous analyses are involvedand it is not subject to the manipulative errors incurred in dealing gravimetrically with minute amounts of material. The method, however,...

Submit Manuscript | http://medcraveonline.com Abbreviations: ILs: Ionic Liquids; CMNPs: Citrate-Coated Magnetite Nanoparticles; TEOS: Tetraethoxyorthosilicate; CPTMS: 3-Cloropropyltrimethoxysilane; IM: Imidazole; XRD: X-Ray Diffraction; FT-IR: Fourier-Transform Infrared Spectroscopy; TGA: Thermal Gravimetric Analysis; VSM: Vibrating-Sample Magnetometer; SEM: Scanning Electron Microscope; TLC: T...

We used a porcine endotoxemic model of acute lung injury to compare extravascular lung water (EVLW) measured by right transthoracic bioimpedance to postmortem gravimetric EVLW measurements. Adult pigs were randomized into control (N = 5) or endotoxin groups [150 microgram/kg Escherichia coli lipopolysaccharide B for 1 hr followed by 3 hr of resuscitation for a thermodilution cardiac output less...