a simple and sensitive high performance liquid chromatographic method with electrochemical detection is described for the quantitative determination of the amoxycillin and clavulanic acid in pharmaceutical dosage forms. separation of sample components occurs on a reversed phase c18 column with a mobile phase consisting of methanol-water-phosphate buffer. for the amperometric detection, the pote...

Aalto University, P.O. Box 11000, FI-00076 Aalto www.aalto.fi Author Pekka Peljo Name of the doctoral dissertation Proton Transfer Controlled Reactions at Liquid-Liquid Interfaces Publisher School of Chemical Technology Unit Department of Chemistry Series Aalto University publication series DOCTORAL DISSERTATIONS 39/2013 Field of research Physical Chemistry Manuscript submitted 10 December 2012...

Wall-to-bed (or wall-to-fluid) heat transfer issues in trickle bed reactors (TBR) has an important impact on operation and efficiency in this category of reactors. In this study, the hydrodynamic and thermal behavior of trickle bed reactors was simulated by means of computational fluid dynamics (CFD) technique. The multiphase behavior of trickle bed reactor was studied by the implementation of ...

abstract: in this study, an analytical method is developed to determine 15 polycyclic aromatic hydrocarbons (pahs) in olive and refined pomace olive oils using hplc coupled with a fluorescence detector. the standardised method of ultrasound-assisted solvent extraction consisted of liquid–liquid extraction with organic solvent and purification on c18 and florisil bonded-phase cartridges was modi...

a rapid, simple and sensitive high-performance liquid chromatography method was developed for determination of ciprofloxacin in plasma by means of ultraviolet detection. ofloxacin was used as an internal standard and separation carried on a novapak c18 column using a mobile phase of 0.01 m phosphate buffer (ph =2.6): methanol (82: 18 v/v). extraction of drug was performed from plasma by liquid-...

since solid-phase and liquid-phase microextraction (spme and lpme) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. however, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. in this way, in recent years, different methods such as ultrason...

the determination region of solubility of methanol with gasoline of high aromatic content was investigated experimentally at temperature of 288.2 k. a type 1 liquid-liquid phase diagram was obtained for this ternary system. these results were correlated simultaneously by the uniquac model. the values of the interaction parameters between each pair of components in the system were obtained for t...

the applicability of hollow fiber-based liquid phase microextraction (hf-lpme) was evaluated for the extraction and preconcentration of loratadine prior to determination by hplc. in order to obtain high extraction recovery, the parameters affecting the hf-lpme including type of organic phase, ph of the source and receiving phases, stirring rate, extraction time and salt addition were studied an...