In this study, ryegrass straw agricultural residue (Lolium multiflorum L.) was employed as an adsorbent material to remove methylene blue (MB) dye from aqueous solutions. Four adsorbents were produced using phosphoric acid and pyrolysis activating agents. The samples analyzed with TGA, FTIR, SEM, XRD techniques. A rapid adsorption of the MB obtained treated 40% H3PO4, reaching equilibrium in 2 ...