Recently helical nanostructures such as nanosprings and nanocoils have drawn great interests in nanotechnology, due to their unique morphologies and physical properties, and they may be potential building blocks in sorts of electromechanical, magnetic, photoelectronic and plasmonic devices at micro/nanoscales. In this report, multi-turns copper nanocoils were synthesized through a modified solv...

Mesoporous TiO2 microspheres assembled from TiO2 nanoparticles with specific surface areas as high as 150 m(2) g(-1) were synthesized via a facile one-step solvothermal reaction of titanium isopropoxide and anhydrous acetone. Aldol condensation of acetone gradually releases structural H2O, which hydrolyzes and condenses titanium isopropoxide, forming TiO2 nanocrystals. Simultaneous growth and a...

nanostructured zinc oxide (zno) materials have received considerable interest from scientists due to their remarkable performance in electronics, optics and photonics. zno nanoparticles were synthesized by co-precipitation method. zno nanoparticles were synthesized using zn(no3)3 and k2co3 precursors. the structure of the obtained product was confirmed by the powder x-ray diffraction (xrd) anal...

Metal organic frameworks (MOFs) are considered an interesting option for hydrogen storage. These materials show an exceptional H2 uptake. Here, Zn3(BTC)2 as MOF was synthesized with a solvothermal method. The phase stability and microstructure of the Zn3(BTC)2 was characterized in terms of their properties and structures, using a number of analytical techniques including FT-IR, XRD, SEM, BET ...

Results of the investigation of the reactions of GaCl3, InCl3 and InI3 with LiNH2 under solvothermal conditions in benzene, which lead to metal nitrides, are reported. GaN is obtained as a cubic phase or as a mixture of cubic and hexagonal phases, depending on temperature. The effect of the addition of surfactants on the formation of GaN was explored. InN products were always contaminated with ...

BaTiO3 nanoparticles were prepared by solvothermal method. The X-ray diffraction (XRD) analysis was used to study the structure and crystallite size of BaTiO3 nanoparticles. The morphology and the size of the BaTiO3 nanoparticles were characterized using scanning and transmission electron microscopy (SEM and TEM). The optical properties were studied using the UV-Visible spectrum in the waveleng...

Mn-doped ZnS nanorods synthesized by solvothermal method were successfully coated with ZnS shells of various thicknesses. The powder X-ray diffraction (XRD) measurements showed the ZnS:Mn nanorods were wurtzite structure with preferential orientation along c-axis. Transmission electron microscopy images (TEM) revealed that the ZnS shells formed from small particles, growing along a-axis orienta...

A novel chemical "top-down" method has been employed to prepare tiny Fe3O4 nanobelts. Uniform Fe3O4 nanobelts were obtained by solvothermal reduction of exfoliated FeOCl layers with the assistance of high polar solvents and a PEO-PPO-PEO stabilizer. We also studied the superparamagnetic properties of Fe3O4 nanobelts, which exhibit a magnetic saturation value as high as ∼53 emu g(-1) at room tem...