A simple chemical bath deposition is used to coat a complex porous ceramic scaffold with a conformal Ni layer. The resulting composite is used as a solid oxide fuel cell electrode, and its electrochemical response is measured in humidified hydrogen. X-ray tomography is used to determine the microstructural characteristics of the uncoated and Ni-coated porous structure, which include the surface...

A three electrodes planar electrochemical sensor, based on CuO nanowires growth “in situ” on Cu working electrode, was fabricated by a simple micromachining technique and employed for the non-enzymatic determination of glucose. The microstructural and morphological characteristics of the modified electrode was investigated by XRD and SEM analysis. Cyclic voltammetry and chronoamperometric measu...

the mechanical properties and microstructural developments of 321 stainless steel during thermomechanicalprocess were investigated. the repetitive cold rolling and subsequent annealing wereconducted to achieve nanocrystalline structure in an aisi 321 stainless steel. heavily cold rolling at−20°c was conducted to form martensite in metastable austenitic steel. the process was followed byannealin...

This work aimed to (a) characterize the microstructure and porosity of human nail and bovine hoof by mercury intrusion porosimetry and SEM image analysis, (b) study the effects of hydration and of N-acetyl-l-cysteine treatment on the microstructure of both membranes, and (c) determine whether the microstructural modifications were associated with changes in drug penetration measured by standard...

In situ reaction was activated in the powder mixture of Al/5 wt.%Fe2O3 by using selective laser melting (SLM) to directly fabricate aluminium metal matrix composite parts. The microstructural characteristics of these in situ consolidated parts through SLM were investigated under the influence of thick powder bed, 75  μm layer thickness, and 50  μm layer thickness in various laser powers and sca...

In this work, the underlying micro-damage mechanisms of randomly oriented short fibre-reinforced composites were revealed based on real internal microstructural characteristics obtained by high-resolution (0.7 μm/pixel) synchrotron radiation X-ray computed tomography (SR-CT). The special 'pore dominant micro-damage processes' were directly observed through SR-CT three-dimensional reconstructed ...

The effects of thermal annealing on the emission and microstructural characteristics of GaAs0.88Sb0.10N0.02/InP multiple quantum well (QW) structures were studied by photoluminescence (PL) spectroscopy and transmission electron microscopy (TEM). The results show that the optimum annealing conditions lead to improved PL intensity accompanied by only a small blue shift, contrasting the behavior o...

The powder and compact characteristics as well as the sintering behaviour of two Ce02-G&03 compositions prepared by the oxalate coprecipitation method are studied as a function of the powder particle size and the pore-size distribution in the powder compacts. Shrinkage was measured at a constant heating rate and the results are compared with those obtained by isothermal sintering experiments. G...

The chemical, physical, and mechanical characteristics of nickel-based superalloys are reviewed with emphasis on the use of this class of materials within turbine engines. The role of major and minor alloying additions in multicomponent commercial cast and wrought superalloys is discussed. Microstructural stability and phases observed during processing and in subsequent elevated-temperature ser...

Fluid-fluid mixtures often possess a fine structure, or morphology, whose length scale is much smaller than the length scale over which the flow field and morphology vary. We define a microstructural variable called the area tensor, which describes the local morphology of such mixtures through volume-averaged size, shape, and orientation characteristics. The area tensor is equivalent to the int...