نتایج جستجو برای: microwave irradiation

تعداد نتایج: 112363  

Journal: :Molecules 2006
Gang Liu Song Yang Baoan Song Wei Xue Deyu Hu Linhong Jin Ping Lu

A simple, efficient, and general method has been developed for the synthesis of various N-aryl heterocylic substituted-4-aminoquinazoline compounds from 4-chloro- quinazoline and aryl heterocyclic amines under microwave irradiation using 2-propanol as solvent. The advantages of the use of microwave irradiation in relation to the classical method were demonstrated.

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 1997
mohammad sadegh khajavi seyed saheb sadat hosseini fatemeh sefidkon

rapid and highly efficient synthesis of 2- or 2,5-substituted 1,3,4-oxadiazoles by the condensation of aryl carboxylic acid hydrazides and orthoesters can be achieved under microwave irradiation using an unmodified commercial over in unsealed vessels.

Journal: :Chemistry 2007
Sung Hwa Jhung Taihuan Jin Young Kyu Hwang Jong-San Chang

Microporous materials, such as silicalite-1 and VSB-5 molecular sieves, have been synthesized by both microwave irradiation (MW) and conventional electric heating (CE). The accelerated syntheses by microwave irradiation can be quantitatively investigated by various heating modes conducted in two steps such as MW-MW, MW-CE, CE-MW, and CE-CE (in the order of nucleation-crystal growth). In the cas...

Journal: :Molecules 2007
Kai Bao Weige Zhang Chuanliang Zhang Yingwei Qu Liang Tian Lan Wu Xiang Zhao Maosheng Cheng

The synthesis of ring-contracted derivatives of erythromycin A via intramolecular transesterification under microwave irradiation of 8,9-anhydroerythromycin A 6,9-hemiketal and its derivatives is described. It was found that microwave irradiation could significantly improve the yields and shorten the reaction times under either solvent-containing (method A) or solvent-free (method B) conditions.

2016
Hiroshi Goto Jun Fukushima Hirotsugu Takizawa

NiMn₂O₄ prepared by conventional heating was irradiated with a microwave H-field using a single-mode cavity under air and magnetic properties of the microwave-irradiated material were investigated. X-ray diffraction and transmission electron microscopy demonstrated that the phase and microstructure are not affected by H-field irradiation. Measurements of the magnetization as a function of tempe...

Journal: :iranian chemical communication 2015
mohammad ali nasseri ali allahresani batol zakeri nasab

microwave assisted green synthesis of α, ά- bis (substituted- benzylidene) alkanones by the crossed- aldol condensation reaction of substituted aryl aldehydes with ketones in the presence of catalytic amount of nbcl5 in good to excellent yields. this reaction is carried out under solvent-free conditions. the results showed that aldehydes bearing electron–donating substituent's on phenyl-ring fa...

Journal: :journal of nanostructures 2013
s. farhadi f. siadatnasab k. jahanara

zno nanorods and nanoparticles have been easily prepared via the decomposition of two simple schiff base zinc (ii) complexes, namely (n,n'–disalicylalethylenediamine)zince(ii) and (n,n'–disalicylalphenylenediamine)zince(ii) under microwave irradiation. the decomposition products of the complexes were characterized by ft-ir, xrd, sem, edx and uv-visible spectroscopy.  ft-ir, xrd and edx results ...

Bagher Goldoost, Ramin karimian

Introduction: hyperthermia using different methods such as microwave and magnetic waves is one of the methods to treat cancer. In this method, iron and magnetic nanoparticles are used to increase the temperature and increase the effect of hyperthermia as auxiliary treatment with chemotherapy and radiotherapy. In this study, the role of iron and magnetic nanoparticles have been ...

Mohammad Sadegh Khajavi Nasser Montazari Seyed Saheb Sadat Hosseini

An efficient synthesis of 3-substituted or 2,3-disubstituted 4(3H)-quinazolinones from benzoxazin-4-ones and primary amines under microwave irradiation in unsealed vessels is described.

Ahmad Ahaabani Ayoob Bazgir, Farzad Bahadoran Naser Safari

Phthalocyanine complexes of Cu, Co, Ni, Fe, Zn, Pd, Pt and Ru have been synthesized from reaction between phthalonitrile and proper metal salts upon exposure to microwave irradiation under solvent-free conditions and considerably reduced reaction times.

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