The absence of residual solvent in metal precursors can be of key importance for the successful preparation of metal complexes or materials. Herein, we describe methods for the quantitation of residual coordinated tetrahydrofuran (THF) that binds to Fe[N(SiMe3)2]2, a commonly used iron synthon, when prepared according to common literature procedures. A simple method for quantitation of the amou...

Single crystals of the new compound Cu2Cd(B20 5) 0 have been prepared by B20 3/V 20 5 flux technique in a closed silver tube. Their structure is isotypic with Cu2Co(B20 5) 0 but its preparation is quite different. X-ray investigations on single crystals led to the space group C |h-P 2 !/c (Nr. 14), a = 339.9(2); b = 1509.8(2); c 927,0(1) pm; ß = 93.19(1)°; Z 4. The structure contains isolated B...

PURPOSE This study examined whether any of a series of segmental and whole-word measures of articulatory competence captured more of the variance in impressionistic ratings of severity of involvement in speech delay. It also examined whether knowing the age of the child affected severity ratings. METHOD Ten very experienced speech-language pathologists rated severity of involvement from conve...

Tourism has become a very important and dynamic sector both in the world economy and particular in the developing countries. Its growth affects not only the activities directly linked to tourism but also other sectors. Tourism is already an important sector in some developing countries and will become so for others. Developing countries have been fast growing in tourism industry terms in the wo...

A comparative study was performed on the initial and final bacillary indexes of 213 multibacillary leprosy patients who received 12 doses (Group 1: 128 patients) or 24 doses (Group 2: 85 patients) of multidrug therapy (MDT/WHO) to measure the effectiveness of the two regimens. All patients were evaluated at treatment baseline, 12 months, and 24 months. The reduction in bacillary levels and mean...

In order to evaluate the graduates attending second-round examination objectively, this study established graduate second-round examination evaluate system based on Analytic Hierarchy Process (AHP) and Fuzzy comprehensive evaluation method. Evaluation indexes in the system included knowledge structure, scientific research ability and comprehensive quality of graduates attending second-round exa...

This paper demonstrates the advantage of combining a ranked output from a fulltext index and another from an index generated using generic summary texts. Our main ndings are as follows: (1) The combination of a fulltext-based run and a summary-based run can signi cantly outperform either alone, especially when the fulltext evidence is emphasized. (2) The primary role of the summary index in the...

The preparation of new Ru(II) complexes incorporating fac-coordinated lutidine-derived CNC ligands is reported. These derivatives are selectively deprotonated by (t)BuOK at one of the methylene arms of the pincer, leading to catalytically active species in the hydrogenation of imines.

This study contributes to the literature on supply chain coordination by coordinating the research and development (R&D) effort, retail price, and inventory decisions. It investigates a real case in the home appliance industry. The main purpose of this study is to examine the optimal values of R&D effort, pricing, and inventory decisions under decentralized and centralized structures. Then, a d...

The preparation of Lanthanon octa-coordinated mixed chelates with different types of ligands is uncommon. Thompson and Loraas [1] have shown the presence of octacoordinated mixed chelates in solution. Recently, Dutt and Sur [2] have actually isolated several mixed tetrakis compounds of La, Pr, Nd, and Sm with three acetylacetone (Acac) molecules, the other ligands being propionylacetone or benz...