نتایج جستجو برای: ray diffraction and micro
تعداد نتایج: 16903940 فیلتر نتایج به سال:
Abstract Aluminum nanoparticles are widely used in various energetic materials, such as pyrotechnics, explosives and propellants.In this research, the thermal behavior of aluminum nanoparticles (prepared by inert gas condensation process) and aluminum microparticles is investigated. The synthesis particles were characterized using Scanning Electron Microscopy (SEM), Particle Size Analysis (...
ZnO and Cu doped[1] (CZO) thin films were prepared by radio frequency sputtering. The structural and optical properties of thin films were investigated using X-ray diffraction (XRD), atomic force microscopy (AFM), optical spectrophotometer, and photoluminescence (PL) techniques. ZnO thin films showed crystalline and micro-stress defects in the crystal lattice. Annealing of CZO thin films increa...
Micro-XRF analysis provides us with elemental maps, which are very useful for understanding the samples under test. Usually, scanning-type elemental mapping is performed. That means, a sample stage is scanned to a fixed X-ray micro beam. XRF analysis is performed at the scanned points, leading to 2D elemental mapping. One of the drawbacks of this technique is the long acquisition time depending...
In this study, Plasma Electrolytic Oxidation (PEO) technique was used for generating ceramic layer on the surface of aluminum alloy AA2024-T6 and the effect of coating time on the electrochemical corrosion behavior, micro-hardness, morphology of coating, and the phase structure was studied. The alloy was coated in 1, 3, 5 and 7 minutes at a constant electrical potential 550 V in a sodium silica...
A new optic system that produces a monochromatic microbeam for both CuKα and CrKα radiation for X-ray diffraction (XRD) has been developed. Multilayer optics technology is a well-known tool to produce a monochromatic micro X-ray beam for XRD. This new optic was combined with a microfocus rotating anode X-ray generator and a cylindrical imaging plate detector to provide a complete dual wavelengt...
for several recent years, syntheses of spherical zeolitic materials, such as S-1, ZSM-5 and Beta, have been reported using an anion exchange resin as macro-templates. Conceptually, these syntheses are based on the use of a colloidal crystal templating process. The advantage of this method is preparation of pure self-bonded zeolite micro/macrostructures. In this paper the synthesis of TS-1 is...
this paper describes day-one beamlines of the iranian light source facility and design concept of powder diffraction and spectromicroscopy beamlines as the most priorities of each synchrotron that cover the research requirements in the fields of physics, chemistry, nano-science, etc. for powder diffraction beamline energy range is 6-30 kev, resolution: 10-4, flux: 1012(ph/s/0.1%b.w.) and spot s...
Calcite crystals were grown from solution with single-crystal dimensions up to 3 mm and doped up to 0.1 at% with Nd ions. Phase purity was verified by powder X-ray diffraction. The concentration of Nd was measured by energy-dispersive spectrometry and Rutherford backscattering spectrometry. Micro X-ray fluorescence mapping of the calcite grains indicates uniform Nd distribution in as-grown crys...
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