This paper presents the retrofit of five conventional distillation trains for the separation of quaternary mixtures of hydrocarbons for feed compositions with high or low content of intermediate components. The retrofit implies the incorporation of liquid or vapour recycle streams among the conventional distillation columns. Each recycle stream removes one condenser or one reboiler. The introdu...

Essential oils are used in a wide variety of consumer goods such as detergents, soaps, toilet products, cosmetics, pharmaceuticals, perfumes, confectionery food products, soft drinks, distilled alcoholic beverages (hard drinks) and insecticides. The world production and consumption of essential oils and perfumes are increasing very fast. Production technology is an essential element to improve ...

A new HIGEE device-rotating zigzag bed (RZB) was developed in the context of process intensification. The RZB is structurally featured by a combinatorial rotor of one series of baffles attached to a rotating disk with another series to a stationary disk. The novel structure of the RZB determines its many advantages over the other HIGEE devices. The RZB is free of dynamic seal, capable of interm...

The continuous fast pyrolysis of soybean oil in a pilot plant was investigated. The experimental runs were carried out according to an experimental design alternating the temperature (from 450 to 600 degrees C) and the concentration of water (from 0% to 10%). The liquid products were analyzed by gas chromatography and by true boiling point (TPB) distillation. A simple distillation was used to o...

A method for deriving reduced dynamic models of one-dimensional distributed systems is presented. It inherits the concepts of the aggregated modeling method of Lévine and Rouchon originally derived for simple staged distillation models and can be applied to both spatially discrete and continuous systems. The method is based on partitioning the system into intervals of steady-state systems, whic...

Thermally coupleddistillation systems (TCDS) havebeenproposed toperformdistillation separation tasks with the incentive of achieving lower energy consumption levels with respect to conventional distillation sequences. In particular, the presence of recycle streams for TCDS schemes has influenced the notion that control problemsmight be expected during the operation of those systemswith respect ...

This paper is about the analysis 0f the liquid discharge by falling film within a distillation tube. Specifically about some flow rates that can be used in this process, when we talk about film ́s discharge and maintenance. This aim of this paper is to study through simulations in CFD (Computational Fluid Dynamics) what influence the feeding flow rate has on the film ́s formation, its stability a...