In previous studies nano sized hydroxyapatite (HA) particles were prepared by solgel or precipitation methods, in which the products were washed by aqueous or non-aqueous liquids to remove impurities or undesired components. The washing is know to modify the surfaces of the cystalline particles. This study evaluated properties of nano HA materials prepared by a spray drying method in which the ...

We report the results of an experimental study to determine influence pressure on diffusion creep in wet olivine. In order observe at high-pressure conditions laboratory strain rates, we prepared ultra-fine grained (0.22–0.72 μm) olivine aggregates both from San Carlos and oxide mixtures using a solgel technique. All samples contain some water (~1000 ppm wt) presumably due adsorption fine-grain...

Electrorheological (ER) properties under oscillatory shear of perchloric acid doped-poly(3-thiopheneacetic acid)/oil (P3TAA/silicone) suspensions have been investigated. The effects of electric field strength, silicone oil viscosity, and particle concentration were investigated. When the electric field strength reaches a critical value, the P3TAA-based ER fluid exhibits transitional behavior be...

High quality manganese oxide thin films with smooth surfaces and even thicknesses have been prepared with a nonaqueous sol-gel process involving reduction of tetraethylammonium permanganate in methanol. Spin-coated films have been cast onto soft glass, quartz, and Ni foil substrates, with two coats being applied for optimum crystallization. The addition of alkali metal cations as dopants result...

nanobiotechnology appears to be an emerging science which leads to new developments in the field of medicine. importance of the magnetic nanomaterials in biomedical science cannot be overlooked. the most commonly used chemical methods to synthesize drugable magnetic nanobeads are co-precipitation, thermal decomposition and microemulsion. however monodispersion, selection of an appropriate coati...

We describe the attempt to synthesize emotional speech with a concatenative speech synthesizer using a parameter space covering not only f0, duration and amplitude, but also voice quality parameters, spectral energy distribution, harmonics-to-noise ratio, and articulatory precision. The application of these extended parameter set offers the possibility to combine the high segmental quality of c...

A simple quantitative approach to enable chemists to compare alternative chemical syntheses on the lab bench with respect to their resource usage and their potential environmental impact is proposed; this may be useful for the systematic design of more sustainable processes. We consider as metrics the mass index S(-1) and the environmental factor E to characterize quantitatively the reaction in...

We present a language to specify syntax guided synthesis (SyGuS) problems. Syntax guidance is a prominent theme in contemporary program synthesis approaches, and SyGuS was first described in [1]. This paper describes concretely the input format of a SyGuS solver.

This paper describes our on-going work in the area of text-tospeech synthesis, specifically on concatenative techniques. Our preliminary work consisted in investigating the current trends in concatenative synthesis and the problems that could arise when we apply the existing state-of-the art solutions to the specific case of European Portuguese. Our ultimate goal is to develop a text-to-speech ...

We demonstrate that isophthalic acid-ended telechelic poly(1,5-cyclooctadiene)s (APCODs) form thermo-reversible gels in non-polar solvent with a unique molecular mechanism for their thermo-reversibility. Like other associative telechelic polymers, A-PCODs form “flower-like” micelles at low concentration and form gels through bridging at higher concentration which exhibit linear viscoelasticity....