نتایج جستجو برای: synthesis condition
تعداد نتایج: 718543 فیلتر نتایج به سال:
The synthesis of the title compound is described. Deprotection of Cis(N-Trityl-3-azido-4-Styryl)-2-azetidinone to Cis-(3-azido-4-styryl)-2-azetidinone was found to be accelerated by the special salt effect under acidic condition
The synthesis of functionalized 2-oxo-2H-coumarin derivatives has been studied by a one-pot reaction of o-hydroxybenzaldehyde, ethyl 2-bromoacetate and triphenylphosphine in the presence of catalytic amount of triethyl amine in EtOAc, water or under solvent free conditions. We have found the best results obtained under solvent free condition.
Silica supported phosphorus pentoxide (P2O5·SiO2) is an efficient catalyst for synthesis of 1,3,5-substituted pyrazoles via the condensation of 1,3-diketones and hydrazines. Simplicity of procedure, mild condition, being solvent-free, high yields, and easy workup are some advantages of this protocol.
An efficient one-pot condensation for the synthesis of 1,8-dioxo-octahydroxanthene is achieved through a condensation of aryl aldehydes and 5,5-dimethyl-1,3-cyclohexandione in the presence of NBS. This method enjoys several advantages such as low cost, simple work up procedure and safe reaction condition. In addition, water was chosen as a green solvent.
An efficient, simple and convenient route is described for the synthesis of biscoumarin (3,3'-(arylmethylene) bis (4-hydroxy-2H-chromen-2-one)) by using of recyclable catalyst TiO2@KSF. In this Method, we synthesis biscoumarin derivatives via 3multi-component reactions (3MCRs) of two equivalent 4-hydroxycoumarin with one equivalent of aromatic aldehydes using 20 mg nano TiO2@KSF as homogeneous ...
Various antibacterial fluoroquinolone compounds were prepared by the direct amination of 7-halo-6- fluoroquinolone-3-carboxylic acids with a variety of piperazine derivatives and (4aR,7aR)-octahydro-1H-pyrrolo[3,4-b] pyridine using Zirconia Sulfuric Acid (ZrSA) nanoparticle, as a catalyst in the presence of ordinary or magnetized water upon reflux condition. The results showed that ZrSA exh...
The present study focused on the synthesis of silver nanoparticles using the aqueous extract of Ulva flexousa (green seaweed). Ten ml of the aqueous extract of alga was mixed with 90 ml of 1mM aqueous AgNO3 solution for reducing of Ag+ ions. The synthesized silver nanoparticles were characterized by UV-Vis spectra, XRD (X-ray diffraction), TEM (Transmission electron microscopy) and FT-IR (Fouri...
the present study concentrates on the synthesis of au nanoparticles (aunps) using aqueous solution of polyvinylpyrrolidone (pvp) and tetrachloroaurate by different methods as thermal, sonochemical and electrochemical reduction. the pvp has been used as a reducing agent and acts as a stabilizer for au nano particles that obtained as principal product. in all synthesis procedures, the active radi...
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