نتایج جستجو برای: thermal gravimetric analysis

تعداد نتایج: 3001115  

Journal: :علوم و تکنولوژی پلیمر 0
مهدی کرمی قهی محمدحسین بهشتی مسعود اسفنده امیرمسعود رضادوست

phenolic resin is among the oldest thermoset resins that have found wide spread applications in several industries, largely due to its high thermal resistance. in this research, room temperature curing of phenolic resin and its reinforced silica composite has been investigated by p-toluene sulphonic acid as a catalyst. mechanical properties of the composites such as impact strength, flexural pr...

2013
K. Mohana Priyadarshini A. Chandramohan T. Uma Devi S. Selvanayagam B. Sridhar

A new charge transfer molecular complex salt of picric acid with m-toluidine was synthesized and the structure confirmed by single crystal X-ray diffraction (XRD) and NMR spectral analyses. Single crystals of m-toluidinium picrate have been grown by slow solvent evaporation solution growth technique using ethanol as the solvent at ambient temperature. The single crystal XRD analysis of MTP salt...

We synthesized CoFe2O4 nanoparticles using heating in various times by simple microwave method at power about 600W. Water, ethylene glycol and their combination were used as solvent. X-ray diffraction pattern(XRD) analysis was performed for evaluation of structural characterization of samples. We also used scanning electron microscopy (SEM) to evaluate the effects of various parameters of heati...

2010
Javad Azizian Hasan Tahermansouri Esmaeil Biazar Saeed Heidari Davood Chobfrosh Khoei

Imidazoles and their derivatives are compounds with chemotherapeutic applications. In this study, we investigated the chemical functionalization of carboxylated multiwalled carbon nanotubes (MWNT-COOH) by 1,2-phenylendiamine. Multiwalled nanotube (MWNT)-benzimidazole was obtained by an MWNT-amide reaction with POCl(3) after 72 hours, which was confirmed by Fourier transform infrared, scanning e...

2012
REZA SOLEYMANI FATEMEH AFSHARI

20 new poly(ester-imide)s and poly(imide-urethane)s structures were synthesized using low temperature solution condensation polymerization. These compounds were optically active, capable of emitting circularly polarized light. The results indicated that the efficiency of the compounds much higher under this synthesis method. Cost effectiveness and short process were other advantages of this syn...

2017
Wenxi Ma Qiaoling Tong Jian Wang Huali Yang Meng Zhang Hailun Jiang Qinghe Wang Yongxiang Liu Maosheng Cheng

A sustainable catalyst for the selective oxidation of benzyl alcohol (BnOH) to benzaldehyde (BzH) was developed by mineralizing Ti(SO4)2 on graphene oxide foam (GOF) surface. The Ti(SO4)2/GOF was characterized by scanning electron microscopy (SEM), energy disperse spectroscopy (EDS), X-ray diffraction (XRD), solid-state NMR (SSNMR), thermal gravimetric analysis (TGA), infrared (IR) and BET anal...

داور, فاطمه, شجاع رضوی, رضا, شیرین‌پرور, شیما, قربانی, سعید, لقمان استرکی, محمدرضا,

In this research, the nanopowders of lanthanum and neodymium co-doped yttria were synthesized by sol-gel combustion method. Citric acid and glycine were used as the gel maker and fuel respectively. The effect of molar ratio of citric acid to glycine on the grain size and morphology was evaluated. The optimized products were characterized by X-ray diffraction (XRD), field-emission scanning ...

We have reported here a simple, low cost preparation of four new adducts from some anthraquinone disperse dyes with functionalized multi-walled carbon nanotubes in the presence of azochromophore. The structural differences between the final products are evaluated by visual dispersion test, UV-Vis Spectroscopy, Fourier transforms infrared, Raman, nuclear magnetic resonance and thermal gravimetri...

2016
BO HONG FANG CHEN GUOXIN XUE Guoxin Xue

Cellulose nanocrystals (CNCs) can be obtained from bamboo pulp by hydrolysis with sulfuric acid. Firstly, the authors conducted a series of experiments under different conditions, and concluded that the optimal parameters were as follows: sulfuric acid concentration 60%, temperature 45 °C, the time is 90 minutes and the solid-liquid ratio is 1:8. Then, transmission electron microscopy (TEM), Fo...

Journal: :Biomacromolecules 2012
Mariko Ago Kunihiko Okajima Joseph E Jakes Sunkyu Park Orlando J Rojas

Lignin-based fibers were produced by electrospinning aqueous dispersions of lignin, poly(vinyl alcohol) (PVA), and cellulose nanocrystals (CNCs). Defect-free nanofibers with up to 90 wt % lignin and 15% CNCs were achieved. The properties of the aqueous dispersions, including viscosity, electrical conductivity, and surface tension, were examined and correlated to the electrospinnability and resu...

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