We use ultraviolet data, acquired with a photodiode-array detector coupled to a reversed-phase liquid-chromatographic system, to identify unknown drugs in plasma samples of acutely poisoned patients. Both retention time and spectra of the peaks obtained with a microbore Hypersil ODS column under gradient elution are compared with a library of approximately 350 compounds. We present our three-ye...

Diamond photoconductive detectors have previously been shown to be suitable for detection of deep ultraviolet nanosecond-scale pulses from excimer lasers, which are to be used in next generation lithographic systems. Using simple test circuitry and low bias voltages easily measurable responses were observed when these detectors were illuminated with laser pulses at typical laser fluence levels....

An on-line automated method for photodegradation studies of isoproturon, diuron, atrazine, fenitrothion, and metoxuron by means of liquid chromatography/mass spectrometry (LC/MS) with particle beam (PB) interface is described. Surface water samples were first spiked with 50 µg/l of each pesticide and then exposed to the radiation of the medium-pressure mercury lamp. Next, in regular intervals o...

Ultraviolet-C (UVC) radiation-based sanitization has globally gained enormous importance in the current COVID-19 (caused by SARS-COV-2 virus) pandemic situation. The effectiveness of radiation is quantified terms ‘radiation dose’, which turn derived from a radiometric parameter ‘irradiance’, measured using UVC radiometer. Metrological traceability irradiance/dose measurement essentially require...

tetracyclines (tcs) are broad-spectrum antibiotics that are used widely in veterinary medicine. the present study was carried out to trace the residues of oxytetracycline (otc) and tetracycline (tc) in pasteurized milk that is marketed in tehran with the use of a high performance liquid chromatography (hplc). ninety milk samples were collected during five sequential days from the products of si...

Tetracyclines (TCs) are broad-spectrum antibiotics that are used widely in veterinary medicine. The present study was carried out to trace the residues of oxytetracycline (OTC) and tetracycline (TC) in pasteurized milk that is marketed in Tehran with the use of a High Performance Liquid Chromatography (HPLC). Ninety milk samples were collected during five sequential days from the products of si...

A rapid, simple and sensitive high-performance liquid chromatography method was developed for determination of ciprofloxacin in plasma by means of ultraviolet detection. Ofloxacin was used as an internal standard and separation carried on a Novapak C18 column using a mobile phase of 0.01 M phosphate buffer (pH =2.6): methanol (82: 18 v/v). Extraction of drug was performed from plasma by liquid-...

A new detector system with high time resolution ~1 ms! has been developed and applied for the continuous measurement of spectra in the vacuum ultraviolet ~VUV! and extreme ultraviolet ~EUV! wavelength region at the fusion plasma experiment Torus Experiment for Technology-Oriented Research ~TEXTOR!. The system consists of an open multichannel-plate ~MCP! detector with subsequent first generation...

A newly developed single quad mass spectrometry (MS) detector was coupled to a ultra-high performance liquid chromatography (UPLC) system and implemented in the routine quality control (QC) and impurity analysis of four therapeutic peptides, namely bleomycin sulfate, tyrothricin, vancomycin HCl and bacitracin, which were selected given their multi-component drug nature and their closely structu...