In this study, a method for extraction and preconcentration of trace amounts of organophosphorus pesticides (OPPs) in environmental water using magnetic solid phase extraction (magnetic-SPE) followed by high performance liquid chromatography (HPLC) with UV detection was developed. The magnetic carbon nanotube adsorbents (Fe3O4/CNT) were synthesized by grafting carbo...

a simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (dllme) was developed for determination and speciation of trace amounts of chromium (cr) by flame atomic absorption spectrometry (faas). in the proposed approach, chloroform and methanol were used as extraction and dispersive solvents. a new schiff's base ligand, bis(2-methoxy benzaldehyde) ethylene d...

in this study, simple and efficient ultrasound-assisted emulsification microextraction (usaeme) combined with gas chromatography-flame ionization detector (gc-fid) was developed for the preconcentration and determination of carbamazepine in biological samples. in this method, the fine droplets of 1-octanol were formed and dispersed in the sample with the help of ultrasonic waves, which accelera...

Various novel techniques including ultrasound-assisted extraction, microwave-assisted extraction and supercritical fluid extraction have been developed for the extraction of medicinal plants in order to shorten the extraction time, decrease the solvent consumption, increase the extraction yield, and enhance the quality of extracts. This review was conducted to introduce and compare the conventi...

A simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (DLLME) was developed for determination and speciation of trace amounts of chromium (Cr) by flame atomic absorption spectrometry (FAAS). In the proposed approach, chloroform and methanol were used as extraction and dispersive solvents. A new Schiff's base ligand, bis(2-methoxy benzaldehyde) ethylene d...

Extraction and determination of naproxen from human plasma were performed using Vortex-Assisted Inverted Dispersive Liquid-Liquid MicroExtraction (VA−IDLLME) and High-Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were ...

Various novel techniques including ultrasound-assisted extraction, microwave-assisted extraction and supercritical fluid extraction have been developed for the extraction of medicinal plants in order to shorten the extraction time, decrease the solvent consumption, increase the extraction yield, and enhance the quality of extracts. This review was conducted to introduce and compare the conventi...

The extraction of Terbium (III)from aqueous nitrate solutions with a supported liquid membrane was investigated using a mixture of di-(2-ethylhexyl phosphoric acid (D2EHPA) and tri-octyl phosphine oxide (TOPO) with a molar ratio 1/0.4. The Hydrophobic Polyvinylidene Fluoride (PVDF) membrane was used as solid support. The sorption process followed pseudo-second-o...

Applying a simple and selective sample preparation procedure prior to instrumental analysis is the most important and crucial step in an analytical process. Up to now, various sample preparation techniques based on solid phase extraction (SPE) systems have been developed to isolate various types of analytes from different matrices. In the method presented for preconcentration and measurement of...