Single-crystalline V(2)O(5)·xH(2)O nanorings and microloops were chemically assembled via an ion-induced chemical spinning route in the designed hydrothermal system. The morphology and structure of products were investigated by means of scanning electron microscopy (SEM) and transmission electron microscopy (TEM). X-ray powder diffraction (XRD) measurement, energy-dispersive X-ray spectroscopy ...

CdSe nanospheres and dendrites have been successfully synthesized via an ionic liquid-assisted hydrothermal synthetic method. The samples are characterized by X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). Our experimental results demonstrate that the CdSe dendrites are obt...

3D hierarchical Bi2S3 architectures have been successfully synthesized via a simple and effective hydrothermal process. The as-prepared Bi2S3 samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorptiondesorption isotherms, and UV-vis diffuse reflectance spectrum (DRS). The observation of field emission sc...

this study reports the simple process to synthesis of cuo/cui nanocomposite in a non-aqueous solution. in the conducted experiments cui and dimethyl sulfoxide (dmso) were used as the precursors. moreover, dmso had role of solvent and ligand simultaneously. in experiments the effects of oleic acid as the particles size modifier, temperature and concentration were investigated. crystalline struct...

Cobalt ferrite nano-powder have been obtained through a hydrothermal method with 2:1 molar ratio of Fe:Co without using any surfactant. X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) were used to consider the structural and morphological properties of CoFe2O4 nano-particles. Also, EDAX spectroscopy applied to evaluate the chemical composition. Results demonstrated that 15 hr hyd...

among different spd techniques, equal channel angular pressing has attracted the most attentions,because of applying large strain to solid bulk materials. in this research, ecap process up to 6passes was carried out on a pure copper and a 6012 al-mg-si alloy with bc route in ecap dieswith φ=120 and ψ=20 and diameter of 20and 10 millimeter respectively. moreover, x-raydiffraction (xrd) system wa...

carbon spheres were fabricated by hydrothermal method and their structural properties were investigated. carbon spheres with average sizes around of 230, 320 and 430 nm were synthesized in different concentration of glucose aqueous solution and different hydrothermal reaction time. the temperature of 180 °c by a hydrothermal reaction was fixed in all of glucose concentration and hydrothermal re...

In this letter, we report on the obtention of hafnium oxide (HfO(2)) nanostructures by the microwave-hydrothermal method. These nanostructures were analyzed by X-ray diffraction (XRD), field-emission gum scanning electron microscopy (FEG-SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDXS), ultraviolet-visible (UV-vis) spectroscopy, and photoluminescence (PL...

Cobalt ferrite nano-powder have been obtained through a hydrothermal method with 2:1 molar ratio of Fe:Co without using any surfactant. X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) were used to consider the structural and morphological properties of CoFe2O4 nano-particles. Also, EDAX spectroscopy applied to evaluate the chemical composition. Results demonstrated that 15 hr hyd...

undoped and mn-doped zno nanoparticles were successfully prepared by the hydrothermal method with different annealing temperature conditions. structural, chemical and optical properties of the samples were studied by x-ray diffraction (xrd), field emission scanning electron microscopy (fesem), uv-vis spectrophotometry and fourier transform infrared (ft-ir) spectroscopy. the phase purity was con...