The solid-phase chemiluminescence analysis of gold on the surface of an anion-exchange resin was studied. A method for the fast determination of gold using flow injection was established. The anion-exchange resin was used as an adsorbent of gold ion in the form of AuCl4-. The cation-exchange resin was used for the on-line separation of cations in the matrix. To obtain the best results, the prec...