The CoFe2O4 nanoparticles have been synthesized by using a stable ferric salt of FeCl3 with a micellar microemulsion method. The normal micelles are formed by sodium dodecyl sulfate (NaDS) in aqueous solutions. The mean size of the nanoparticles can be controlled from less than 4 nm to about 10 nm through controlling the concentrations of the reagents. The neutron diffraction in combination wit...

We report the effect of a polyol-mediated annealing on nickel ferrite nanoparticles. By combining X-ray fluorescence spectroscopy, diffraction, and 57 Fe Mössbauer spectrometry, we showed that whereas as-prepared nanoparticles (NFO) are stoichiometric, annealed ones (a-NFO) not, since Ni 0 -based crystals precipitate. Nickel depletion from spinel lattice reduction in polyol solvent accompanied ...

the dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. cu and ni unites nanocatalyst powders sithcomposition of caned], and nife204 were synthesized by a sol-gel auto catalnic combustion process. themolar ratio between metal ions and urea was 11.2. the sob gel process was done at 8...

Ferrite nanoparticles were synthesized at around 4°C~25°C and coated during the synthesis process with biocompatible and biodegradable polymers, dextran or chitosan. The size of ferrite nanoparticles was determined to be 7.51nm by DLS (Dynamic Light Scattering) and TEM (Transmission Electron Microscope). The size of coated nanoparticles was increased up to 128.6nm and 67nm for dextran and chito...

Nanocrystalline nickel ferrite (NiFe2O4) has been synthesized from a stoichiometric mixture of oxides NiO and α-Fe2O3 in a high energy planetary mill. A post milling annealing at 350 °C was used to improve the solid state reaction. The obtained powders were investigated by X-ray diffraction, magnetic measurements, scanning electron microscopy, X-ray microanalysis, differential scanning calorime...

Global warming persuades researchers to improve the effectiveness of renewable energy technologies, such as H2 production by methane steam reforming (MSR) an endothermic process. Herein, a nanocatalyst based on open-cell nickel foam 40 (pore per inch) with high thermal conductivity was prepared. The synthesized chemical stepwise synthesis approach, pre-treatment, pulsed electrocodeposition Ni-A...

The magnetic nanoparticle composite NiFe2O4 has traditionally been studied for high-frequency microwave absorption with marginal performance towards low-frequency radar bands (particularly L and S bands). Here, NiFe2O4 nanoparticles and nanohybrids using large-diameter graphene oxide (GO) sheets are prepared via solvothermal synthesis for low-frequency wide bandwidth shielding (L and S radar ba...

Hydrotalcite nanoparticles were synthesized by co-precipitation of aqueous Mg(NO(3))(2)·6H(2)O and Al(NO(3))(3)·9H(2)O in the presence of urea and subsequent microwave-hydrothermal treatment. The nanoparticles were activated with saturated aqueous Ca(OH)(2), and used to hydrolyze cellulose. A maximum hydrolysis yield of 47.4% with high glucose selectivity (85.8%) was achieved at 423 K. The nano...

A Pd/α-Al2O3 nanocatalyst with ultra-low Pd loading exhibits high activity and stability for CO oxidative coupling to dimethyl oxalate, which was prepared by a Cu(2+)-assisted in situ reduction method at room temperature. The small size and high dispersion of Pd nanoparticles facilitated by Cu(2+) ions are responsible for the excellent catalytic activity.