By simply crushing mineral grains, suspending the powder in a liquid, and dispersing the suspension on a suitable substrate, it is possible to collect adequate compositional and structural information to identify an unknown phase using a scanning electron microscope (SEM) equipped with an energydispersive X-ray spectrometer (EDS) and an electron backscatter diffraction system (EBSD). This techn...

in this work firstly mgfe2o4 nanoparticles were synthesized via a microwave-assisted method. the product was calcinated at 900 ºc for 2h. at the second step zinc oxide shell was synthesized on the ferrite under ultrasonic waves. properties of the product were examined by x-ray diffraction pattern (xrd), scanning electron microscope (sem) and fourier transform infrared (ft-ir) spectroscopy. vibr...

Mixed morphologies of Ga-doped Zinc Oxide (ZnO) nanostructures are synthesized by vapor transport method. Systematic scanning electron microscope (SEM) studies of different morphologies, after periodic heat treatments, gives direct evidence of sublimation. SEM micrographs give direct evidence that morphological defects of nanostructures can be removed by annealing. Ultra Violet (UV) and visible...

The present paper investigated a preparation of Nano sized Mg0.2Fe0.8O by eco-friendly chemical combustion synthesis using magnesium and iron nitrates as oxidizers and the glycine as a fuel to drive the reaction. Powder characterization was carried out by X-ray diffraction (XRD) to estimate crystallite size, Particle Size Analyzer (PSA), Thermal gravimetric analyzer (TGA) for determining sample...

We report the nanostructures and gas-sensing properties of Zinc oxide nanosheets prepared by hydrothermal method. In particular, needlelike Zinc oxide was also prepared for comparison. The morphology and structural properties were investigated using X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscope (TEM). Subsequent gas-sensing measurement between ...

cadmium oxide (cdo) nanoparticles were prepared by precipitation method using cadmium acetate and ammonia solution. presence of chemical species, were verified by fourier transform infra red (ftir) spectrum. from x-ray diffraction (xrd) spectrum the particle size, d-spacing value and structure of the nanoparticle were analysed. size of the nanoparticles and the elemental composition were detect...

Polypropylene/Multiwall carbon nanotubes/Montmorillonite (PP/MWNTs/MMT) hybrid nanocomposites were prepared by using twin-screw extruder incorporating the polypropylene grafted maleic anhydride (PP-g-mA) as compotibilizer is used for better dispersion of nanoclay in the polymer matrix. The effect of MWNTs and MMT on the polypropylene matrix was investigated in terms of mechanical properties of ...

Effects of laser shock processing (LSP) on the cavitation erosion resistance of laser weldments were investigated by optical microscope (OM), scanning electron microscope (SEM) observations, roughness tester, micro hardness tester, and X-ray diffraction (XRD) technology. The morphological microstructures were characterized. Cumulative mass loss, incubation period, erosion rate, and damaged surf...

A method produced to preparate the CdS Cadmium sulfer using the paraffin oil instade the Olyelamine acid since it is toxic solution. The optical properties were measured by using the absorption and photoluminescence spectrum where the energy gap is about 2.8 eV. The structure properties of the prepared nanoparticles was carried out by measuring the X-ray diffraction which show the hexagonal str...

We designed and built a combination of a scanning tunneling microscope ~STM! and a scanning electron microscope ~SEM! which is working under ultrahigh vacuum conditions ~base pressure typically 7 • 10 mbar!. The SEM is ideally used for surveying the sample and to control the STM tip positioning, while the STM extends the resolution range into the atomic scale. The design concept allows moving t...