Using a portable total reflection X-ray fluorescence spectrometer, a sample containing 100 pg each of 3d transition metals, 500 pg of As, and 1 ng each of Sr, Y, and Zr is measured. Although non-monochromatic X-rays from a 5 W X-ray tube (Tube voltage: 25 kV) are used, the trace amounts of these elements are detected. This portable spectrometer is applied to analysis of river water, a leaching ...

Measurements by instruments on spacecraft have significantly advanced cosmochemistry. Spacecraft missions impose serious limitations on instrument volume, mass, and power, so adaptation of laboratory instruments drives technology. We describe three examples of flight instruments that collected cosmochemical data. Element analyses by Alpha Particle X-ray Spectrometers on the Mars Exploration Rov...

We developed a single-shot X-ray spectrometer for wide-range high-resolution measurements of Self-Amplified Spontaneous Emission (SASE) X-ray Free Electron Laser (XFEL) pulses. The spectrometer consists of a multi-layer elliptical mirror for producing a large divergence of 22 mrad around 9070 eV and a silicon (553) analyzer crystal. We achieved a wide energy range of 55 eV with a fine spectral ...

We present a study of the X-ray coronal emission from the active binary VY Ari, using data from both the Low EnergyConcentrator Spectrometer (LECS) and theMediumEnergy Concentrator Spectrometer (MECS) instruments on-board the X-ray satellite BeppoSAX. Using these instruments, the Xray spectrum of VY Ari can be studied across two full decades of energy, from 0.1 to 10 keV. The spectrum is well f...

The Chandrayaan-2 Large Area Soft X-ray spectrometer (CLASS) is due to be launched by the Indian Space Research Organisation (ISRO) in 2014. It will map the elemental composition of the lunar surface, building on the Chandrayaan-1 X-ray spectrometer (C1XS) heritage. CLASS will use an array of e2v technologies CCD236 swept charge devices (SCD) providing an active detector area of approximately 6...

A curved-crystal x-ray emission spectrometer has been designed and built to measure 2-5 keV x-ray fluorescence resulting from a core-level excitation of gas phase species. The spectrometer can rotate 180 degrees, allowing detection of emitted x rays with variable polarization angles, and is capable of collecting spectra over a wide energy range (20 eV wide with 0.5 eV resolution at the Cl K edg...

A portable instrument for two-dimensional X-ray fluorescence imaging was assembled with an X-ray source using a pyroelectric crystal, which was driven by a 9-V dry battery, a Si-PIN detector, a slit, and pulse motors. Line scanning for a mug and a knife-edge-scan of an iron sheet were carried out using this spectrometer. The sensitivity of the spectrometer was sufficient for elemental analysis ...

X-ray crystallography at third-generation synchrotron sources permits tremendous insight into the three-dimensional structure of macromolecules. Additional information is, however, often required to aid the transition from structure to function. In situ spectroscopic methods such as UV-Vis absorption and (resonance) Raman can provide this, and can also provide a means of detecting X-ray-induced...

Photon and neutron inelastic scattering spectrometers are microscopes for imaging condensed matter dynamics on very small length and time scales. Inelastic X-ray scattering permitted the first quantitative studies of picosecond nanoscale dynamics in disordered systems almost 20 years ago. However, the nature of the liquid-glass transition still remains one of the great unsolved problems in cond...

Amorphous Co1-xPx alloy nanowire arrays with different sizes and 6.8 wt% x 9.9 wt% were fabricated in an anodic aluminum oxide film by electrodeposition. Transmission electron microscopy, selected area electron diffraction, X-ray fluorescence spectrometer, inductively coupled plasma-atomic emission spectrometer, X-ray diffraction spectrometer and vibrating sample magnetometer are employed to st...