نتایج جستجو برای: solvent free microwave extraction

تعداد نتایج: 758549  

Journal: :Journal of oleo science 2017
Himanshu S Shukla Amit Pratap

The present work deals with comparison of microwave assisted extraction to that of conventional solvent extraction for the extraction of rice bran oil (RBO); focusing on extraction yield and oil composition. Microwave assisted extraction act as a green process over other method and proved that it is effective method for extraction of oil. The investigation also focuses on the study of functiona...

Ahmad Ahaabani Ayoob Bazgir, Farzad Bahadoran Naser Safari

Phthalocyanine complexes of Cu, Co, Ni, Fe, Zn, Pd, Pt and Ru have been synthesized from reaction between phthalonitrile and proper metal salts upon exposure to microwave irradiation under solvent-free conditions and considerably reduced reaction times.

Journal: :Journal of analytical toxicology 2007
Purificación Fernández Marta Lago Rosa Antonia Lorenzo Antonia María Carro Ana María Bermejo María Jesús Tabernero

A sample preparation procedure using microwave energy is proposed for the determination of morphine, 6-acetylmorphine, codeine, cocaine, cocaethylene, benzoylecgonine, methadone, and 2-ethylene-1,5-dimethyl-3,3-diphenylpyrrolidine in human plasma. A screening asymmetrical factorial design was used to identify the most suitable extraction conditions as regards solvent, temperature, and extractio...

2012
Huang Guolin Shi Jeffrey Zhang Kai Huang Xiaolan

Microwave-assisted extraction of pectin from lemon peels by using ionic liquid as alternative solvent was investigated. The extracted pectin was detected by Fourier transform infrared spectra. The extraction conditions were optimized through the different experiments in conjunction with the response surface methodology. A pectin yield of 24.68 % was obtained under the optimal parameters: the ex...

2012
Baya Berka-Zougali Mohamed-Amine Ferhat Aicha Hassani Farid Chemat Karim S. Allaf

Two different extraction methods were used for a comparative study of algerian myrtle leaf essential oils: solvent-free-microwave-extraction (SFME) and conventional hydrodistillation (HD). Essential oils analyzed by GC and GC-MS presented 51 components constituting 97.71 and 97.39% of the total oils, respectively. Solvent-Free-Microwave-Extract Essential oils SFME-EO were richer in oxygenated c...

Journal: :Molecules 2011
En-Qin Xia Bo Cui Xiang-Rong Xu Yang Song Xu-Xia Ai Hua-Bin Li

In this paper, microwave-assisted extraction (MAE) of oxymatrine from Sophora flavescens were studied by HPLC-photodiode array detection. Effects of several experimental parameters, such as concentration of extraction solvent, ratio of liquid to material, microwave power, extraction temperature, and extraction time on the extraction efficiencies of oxymatrine were evaluated. The optimal extract...

2014
C. H. Wright Peng Wang Chaoyang Ma Shangwei Chen Song Zhu Zaixiang Lou Hongxin Wang

Purpose: To develop a more green, efficient and low cost process for the extraction of steroidal saponins from Dioscorea Zingiberensis C. H. Wright. Methods: Six kinds of ionic liquids with different cations and anions were evaluated. In addition, the extraction parameters of the ionic liquid based ultrasonic/microwave extraction were studied. In order to quantify the total saponin content accu...

Journal: :The Analyst 2013
Dong-Yang Zhang Xiao-Hui Yao Ming-Hui Duan Meng Luo Wei Wang Yu-Jie Fu Yuan-Gang Zu Thomas Efferth

A novel negative pressure and microwave assisted extraction technique (NMAE) was first proposed and applied for extraction of phenolic compounds from pyrola. [C₄MIM]BF₄ aqueous solution was selected as extraction solvent. Optimal extraction conditions were microwave power 700 W, negative pressure -0.07 MPa, temperature 40 °C, liquid-solid ratio 20 : 1, ionic liquid (IL) concentration 0.5 M, ext...

2015
Mojtaba Delfanian Reza Esmaeilzadeh Kenari Mohammad Ali Sahari

The aim of present study was to compare the effects of ultrasound-assisted and microwave-assisted extraction with solvent extraction method on antioxidant activities of jujube (Ziziphus mauritiana Lam.) leaf extracts in stability of sunflower oil during deep frying. The antioxidant activities of the extracts were evaluated by using 2, 2-diphenyl-1-picrylhydrazyl (DPPH˙) radical scavenging and β...

Journal: :the iranian journal of pharmaceutical research 0
shiva masoudi - jila abbassi my phd student

the essential oils obtained by hydrodistillation (hd), steam distillation (sd) and solvent free microwave extraction (sfme) from the stems and flowers of tanacetum tenuisectum (boiss.) podl., which is endemic to iran,were analyzed by gc and gc/ms.camphor (26.9 %, 27.2% and 25.5%), borneol (12.6%, 11.5% and 7.6%) and 1, 8-cineole (7.9%, 13.2% and 11.3%) were the main constituents of the hd, sd a...

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