in this research, a single-stage low-temperature hydrothermal synthesis route was successfully developed for preparation of iron disulfide. the prepared powder was characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). these analyses showed that nanoparticles were well crystallized, pyrite was the main product and the shape of crystals was nanorod. also, the influences...

In the present study, amorphous tricalcium phosphate (TCP) has been synthetized by a wet route to obtain low temperature ?-TCP at 650 °C (LT-?TCP) and compare its structural, physical–chemical thermal properties with those of obtained conventional solid-state reaction method 1400 (HT-?TCP). Even if no significant differences were observed concerning values lattice parameters measured Rietveld r...

an efficient, simple and convenient route is described for the synthesis of biscoumarin (3,3'-(arylmethylene) bis (4-hydroxy-2h-chromen-2-one)) by using of recyclable catalyst tio2@ksf. in this method, we synthesis biscoumarin derivatives via 3multi-component reactions (3mcrs) of two equivalent 4-hydroxycoumarin with one equivalent of aromatic aldehydes using 20 mg nano tio2@ksf as homogen...

silver nanoparticles (agnps) are amongst the most investigated materials in nanotechnology in view of their unique physio-chemical features and applications in restorative science. their progressive usages in different fields of science besides some predominant restrictions with conventional methods for their synthesis have demanded analysts to discover green courses for their creation. biologi...

In the following research, Lead magnesium niobate relaxor ferroelectric (PMN-PZT) ceramic powders were synthesized using the combustion method grand urea as the fuel for the first time. The starting materials used were lead nitrate, magnesium acetate, niobium oxide, zirconium nitrate, titanium oxide.     The raw materials were first mixed using the general formula of (1-x)Pb(M...

in the present work, the effect of ca(no3)2.4h2o and (nh4)2hpo4 primary solutions as the beginning materials in synthesis of a calcium phosphate phase, was examined. so, we investigated the wet chemical reactions in solution at different temperatures by a hydrothermal condition aimed at hydroxyapatite (ca10(po4)6(oh)2); (hap) synthesis. the powders were investigated by xrd,sem, fe-tem, hrtem, e...

reaction between aromatic aldehydes and 3–methyl-1-phenyl-2-pyrazoline-5-one catalyzed by nano-sio2/hclo4 in water under reflux provided a simple and efficient route for the synthesis of 4-((5-hydroxy-3-methyl-1-phenyl-1h-pyrazol-4-yl)(aryl)methyl)-3-methyl-1-phenyl-1h-pyrazol-5-ol derivatives in high yields.

Developing colloidal plasmonic nanomaterials with high carrier density that show optical resonances and photochemical activity extending from the visible to mid-infrared (MIR) ranges remains a challenging pursuit. Here, we report fabrication of titanium nitride (TiN) nanobars obtained using two step procedure based on wet chemical route synthesis TiO2 nanowires their subsequent temperature anne...