biocl microflowers were synthesized using bismuth nitrate pentahydrate and sodium chloride by microwave (mw) assisted synthesis method for 23 minutes at 180 w. scanning electron microscopy (sem) studies revealed a unique morphology of flower-like assemblies comprised of nanosheets. the x-ray diffraction (xrd) pattern showed that a highly pure and crystalline phase has been obtained. the energy ...

Aerosol-assisted chemical vapour deposition (AACVD) of Cd[(SePiPr2)2N]2 is shown to deposit cadmium selenide and/or cadmium phosphide on glass substrates, depending upon the growth conditions. The phase, structure, morphology and composition of the films were characterised by X-ray powder diffraction (XRD), scanning electron microscopy, energy dispersive X-ray analysis and X-ray photoelectron s...

A facile co-precipitation method for the synthesis of well-dispersed NdFeO3 nanocrystals is developed in the presence of octanoic acid as surfactant. Co-precipitation can produce fine, high-purity, stoichiometric particles of single and multicomponent metal oxides. The product is characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microsc...

core-shell 12-tungstophosphoric acid/tio2 (hpw/tio2) nanoparticles at 10 and 20% of hpw have been synthesized by simple in-situ sol- gel method. characterization of the samples was carried out by x-ray diffraction (xrd), scanning electron microscopy (sem), fourier transform infrared (ftir). the x-ray diffraction patterns of as prepared solid samples, indicated characteristic peaks of titania wi...

Mn-doped nanocrystalline ZnO particles have been successfully synthesized at low temperature (80 ̊C) by the coprecipitation method using zinc sulfatehepta hydrate and NaOH. The structural and magnetic properties have been characterized using X-ray diffraction (XRD), Energy dispersive x-ray, vibrating sample magnetometer and electron spin resonance. XRD measurements revealed that the sample posse...

in this work firstly fe2o3 nanoparticles were synthesized via a simple chemical method. properties of the product were examined by x-ray diffraction pattern (xrd), scanning electron microscope (sem) and fourier transform infrared (ft-ir) spectroscopy. vibrating sample magnetometer (vsm) shows nanoparticles exhibit ferromagnetic behavior. to continue some of the 2-naphthol condensed 1,3-oxazinon...

According to circumstance of kerman sarcheshmeh cooper complex that its anode slime is mainly consisted of Cu, Ag, Au, Pb and Se. In this work, recovery of silver from anode slime and subsequent synthesis of silver nanoparticles from leaching solution was made. Silver was separated from anode slime by using of HNO3 and HCl. X-Ray fluorescence spectroscopy (XRF) was used to characterize anode sl...

According to circumstance of kerman sarcheshmeh cooper complex that its anode slime is mainly consisted of Cu, Ag, Au, Pb and Se. In this work, recovery of silver from anode slime and subsequent synthesis of silver nanoparticles from leaching solution was made. Silver was separated from anode slime by using of HNO3 and HCl. X-Ray fluorescence spectroscopy (XRF) was used to characterize anode sl...

SiO2/ZnS core/shell nanostructures have been synthesized at room temperature by a simple wet chemical method. The prepared materials are characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), infrared spectroscopy (IR), UV–vis spectroscopic and transmission electron microscopy (TEM) studies. X-ray diffraction pattern exhibits peaks correspond to the cubic phase of ZnS. Th...

A bulk single crystal sample of cadmium telluride (CdTe) was irradiated with a ~3 mJ/cm infrared femtosecond laser and analyzed with time-resolved X-ray diffraction (XRD) performed on an in-air tabletop designed for an extremely short pulsed X-ray source. The integrated intensity of Kα XRD lines from the CdTe (111) plane was decreased by 4%–5% in the time scale of ~200 ps. The changes in integr...