Synopsis The application of zirconia ceramics for the dental restorations and dental implants has increased. However the weak performance of the veneering porcelains and low adhesion to the zirconia framework were reported. In this study, the micro-structure, elemental distribution and crystal phase around the interface between zirconia and veneering porcelain were estimated using SEM-EDS (ener...

In the present investigation, Bambusa bambos was used for optimization of enzymatic pretreatment and saccharification. Maximum enzymatic delignification achieved was 84%, after 8 h of incubation time. Highest reducing sugar yield from enzyme-pretreated Bambusa bambos was 818.01 mg/g dry substrate after 8 h of incubation time at a low cellulase loading (endoglucanase, β-glucosidase, exoglucanase...

In this letter, we report on the obtention of hafnium oxide (HfO2) nanostructures by the microwavehydrothermal method. These nanostructures were analyzed by X-ray diffraction (XRD), field-emission gum scanning electron microscopy (FEG-SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDXS), ultraviolet–visible (UV–vis) spectroscopy, and photoluminescence (PL) m...

The corrosion inhibition of mild steel in 0.5 M H2SO4 solution has been investigated using electrochemical methods, X-ray diffraction (XRD) and scanning electron microscope (SEM). The adsorption and inhibition action of acid corrosion of mild steel using cetyltrimethylammonium bromide (CTABr) and different halides (NaCl, NaBr and NaI) has shown synergetic effect. The results showed that the pro...

Abstract: TiO2 thin films were prepared by spray pyrolysis technique at a substrate temperature of 350C under optimum conditions. Films have uniform thickness varying from 0.3–6 μm and good adhesion to substrate. The films were characterized by XRD, SEM and EDAX measurements. XRD profile shows poly crystalline nature of films. As deposited films have anatase phase. Transformation from anatase t...

The alloying and phase formation in Ni-Hf samples with 0.2-, 2-, and 5-at.% Hf were studied by X-ray diffraction (XRD) technique and scanning electron microscopy (SEM). Both characterization methods, XRD and SEM, reveal the presence of the HfNi5 phase (fcc structure) where the excess Ni atoms are present in the form of Ni or Ni-rich segregations in the sample containing 5-at.% Hf. The sample wi...

The surface and optical properties of black chrome films prepared by two different electrochemical baths were characterized. The black chrome films have been deposited on bright nickel substrates by electroplating technique. The surface morphology and phase structure of the films were investigated by using scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. The chemica...

In the Present work structural, morphological and compositional properties of ZnO nanopowders synthesized using Zinc nitrate and NaOH using sol-gel process were reported. The synthesized nanopowders were further analyzed using X-Ray Diffraction (XRD), Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR) spectroscopic characterizations. Crystalline size and Lattice strain det...

Nanocrystalline Se0.8Te0.2 films were grown on quartz substrates by using thermal evaporation technique. Structural and optical properties of as-grown and annealed samples were investigated with XRD, SEM and UV-visible spectroscopy. The x-ray diffraction pattern at room temperature shows that the sample are formed in single phase with monoclinic crystal symmetry having space group Cm. Surface m...

The protective performance of a sand particle-modified enamel coating on reinforcing steel bars was evaluated in 3.5 wt% NaCl solution by electrochemical impedance spectroscopy (EIS). Seven percentages of sand particles by weight were investigated: 0%, 5%, 10%, 20%, 30%, 50% and 70%. The phase composition of the enamel coating and sand particles were determined with the X-ray diffraction (XRD) ...