Cobalt-free, single crystal layered-oxide positive electrode materials like Li 1+x [Ni 0.6 Mn 0.4 ] 1−x O 2 (NM64) have received recent interest because of their low cost, high-voltage stability, and good cycle life. In this work, NM64 is successfully produced with a simple all-dry synthesis process that requires no water, intermediate chemicals, produces little waste. The synthesized has ≤ 4% ...