نتایج جستجو برای: differential thermal analysis dta

تعداد نتایج: 3216137  

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2006
sayed mohammad taghi sadeghi

ionomers are generally described by copolymers having either acrylic or methacylic acid as one component and the other component is mostly either ethylene or styrene. the objective of this research was to study the thermal behaviour and stability of ionomers of styrene with some alkali metal acrylates. these materials have been synthesized by neutralization of the respective copolymer containin...

Journal: :iranian journal of pharmaceutical sciences 0
hossein najafi department of materials science and engineering , sharif university of technology, tehran, iran, ziarat ali nemati department of materials science and engineering , sharif university of technology, tehran, iran, zahra sadeghianb oil research center, tehran, iran nafiseh sohrabi department of materials science and engineering , sharif university of technology, tehran, iran

this article describes the preparation and analysis of nano hydroxyapatite (ha) films on stainless steel 316l through sol-gel technique. the process started with preparation of a nitrate and phosphate sol. after aging the sol for 24 h at room temperature a ss316 substrate was dip-coated and heat-treated at 350 to 450 °c for different times in air. the coating phase and structure on substrate we...

Ghasemi Siani, , Karimi Shahraki, ,

The Haft Sandogh alunite deposit is located in the northwest of Takestan (about 60 Km west of Qazvin), and is a part of large Takand alunite deposit. Mineralogical and field study reveal that there is a zonation in the alteration zones of the Haft Sandogh deposit and surrounding area including silica zone in the central part, and quartz-alunite (quartz alunite), kaolinite and propylitic formed ...

2013
Eva ZEMANOVÁ Eva KOŠŤÁKOVÁ Karel KLOUDA

This work describes the application of oxo-derivatives of fullerene C60 and pristine fullerene as a nanocomposite in polymerous nanofibres. In this work we used oxofullerene derivative, of which preparation was presented by the authors of the State office for nuclear safety (Prague) on Nanocon 2009 and on Nanocon 2010 [1, 2]; there was presented its application in vivo as a radioprotective agen...

2010
Y. C. Sharma Bhaskar Singh John Korstad

Recycled chicken eggshells after calcination have been used as a nonconventional heterogeneous catalyst for biodiesel synthesis from karanja oil from the pongam tree (Pongamia pinnata). The catalyst was characterized on X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, and differential thermal analysis/thermogravimetric analysis (DTA/TGA). The formation of the calcium oxi...

2003
Krishnankutty-Nair P. Kumar Klaas Keizer

Textural evolution in sol-gel derived nanostructured unsupported titania membranes has been studied using differential scanning calorimetry (DSC), differential thermal analysis (DTA), thermal gravimetry (TG), X-ray diffraction (XRD) and N, adsorption. The anatase-to-rutile phase transformation kinetics were studied using the Avrami model. The precursor gel had a surface area of ca. 165 m2 g-', ...

Journal: :Chemical & pharmaceutical bulletin 1999
N Nawar N M Hosny

Coordination compounds of some transition metal ions with 2-acetylpyridene-o-hydroxybenzoylhydrazone (APo-OHBH) were synthesized. Their structures have been characterised by elemental analyses, electrical conductance, magnetic moments (at 25 degrees C) and spectral (IR, UV, NMR) studies. The fast atom bombardment (FAB) method was used for obtaining mass spectra of the positive ion FAB studies o...

In this study, molybdenum-copper/alumina nano composite was synthesized with mechano-chemical method using high energy planetary ball milling. The molybdenum oxide, copper oxide and aluminum powder were used as starting materials and reaction appeared to occur through a rapid combustion reaction process. The evaluation of powder particles after different milling times was studied by X-ray diffr...

امیرآبادیزاده, احمد , عربی, هادی , علیخان‌زاد, سیما ,

 In this paper the effect of ammonium hydroxide addition to the solution of metallic oxide on sol gel preparation process of YBCO is studied with differential thermal analysis, thermal graviometry and X-ray diffraction. Two samples with and without ammonium hydroxide. Ammonium hydroxide prevents both barium nitrate precipitate during the gel preparation and also unwanted reaction as well as inc...

داور, فاطمه, شجاع رضوی, رضا, شیرین‌پرور, شیما, قربانی, سعید, لقمان استرکی, محمدرضا,

In this research, the nanopowders of lanthanum and neodymium co-doped yttria were synthesized by sol-gel combustion method. Citric acid and glycine were used as the gel maker and fuel respectively. The effect of molar ratio of citric acid to glycine on the grain size and morphology was evaluated. The optimized products were characterized by X-ray diffraction (XRD), field-emission scanning ...

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