Distillation column is one of the key elements in the process of chemical industries, which is having nonlinear, multivariable and non-stationary characteristics. The conventional controller like PID provides ineffective control action for nonlinear system. This paper deals the design of the model based predictive controller to control composition of the Bubble cap distillation column consists ...

In this work, the use of heteroazeotropic distillation for separation of thermally instable substances is discussed. A new process has been developed and analysed, which makes use of the fact that the boiling temperature of a heteroazeotrope is always lower that that of its constituents. Three phase distillation is characterised by the fact that two liquid phases and a vapour phase coexist in t...

The issues raised in advanced process control applications lead control engineers to be aware of the need of integrating advanced information processing capabilities in the process control loop. In this paper a SIMULINK based tool has been developed for analysis and design of multivariable neural based control systems. This tool has been applied to the control of a high purity distillation colu...

The feasibility of a novel multivessel batch distillation–decanter hybrid for simultaneous separation of ternary heterogeneous azeotropic mixtures is addressed both theoretically and by simulations. The multivessel column is operated as a closed system without product withdrawal and the three components are accumulated in the vessels during one closed operation. The closed mode (total reflux) o...

Anefficient algorithmisdeveloped for solving the systemofdifferential algebraic equations (DAE)describing the dynamics of a reactive distillation (RD) column using the equilibrium tray model. Unlike existing eceived in revised form 23 January 2009 ccepted 27 January 2009 vailable online 4 February 2009 eywords: eactive distillation algorithms, the rate of change of tray specific enthalpy is obt...

There has been much discussion in the literature regarding whether column profiles can cross distillation boundaries and by how much. The traditional crossing of boundaries demonstrated by Wahnschafft et al. (1993) represents a very constraint case and was of academic interest only as the operating region for columns was small. The goal of this paper is to show how the design by using column se...

An inferential feedforward control strategy is developed and applied to a simulated distillation column. In this control strategy, the effects of disturbances on the primary process variables (top and bottom compositions) are inferred from uncontrolled secondary process variables (tray temperatures) which can be easily measured. The proposed strategies are particularly useful when disturbances ...

The paper presents a detailed analysis of the dynamic behavior of a reactive distillation column. A control relevant dynamic model is derived using firstprinciples modeling and it is used to study the dynamic behavior of the process at high and low purity operating regimes. The results are used to analyze the performance of linear and nonlinear model predictive control in comparison to coupled ...

Production of ethyl dodecanoate (biodiesel) using lauric acid and methanol with a solid acid catalyst of sulfated zirconia is studied by using two distillation sequences. In the first sequence, the methanol recovery column follows the reactive distillation column. In the second sequence, the reactive distillation and methanol recovery columns are thermally coupled. Thermally coupled distillatio...