Background:: Organic solvents play an indispensable role in most of the radiopharmaceutical production stages. It is almost impossible to remove them entirely final formulation product. Objective:: In this presented work, analytical method by gas chromatography coupled with flame ionization detection (GC-FID) has been developed determine organic samples. The effect injection hold time, temperat...

The defensive secretion of Parectatosoma mocquerysi, a walkingstick insect from Madagascar, was determined to contain glucose, water, and a new monoterpene, parectadial, (4S)-(3-oxoprop-1-en-2-yl)cyclohex-1-enecarbaldehyde. Here, we describe the elucidation of parectadial's molecular structure and absolute configuration via microsample NMR technology, GC-MS, CD, chiral GC-FID, and synthesis fro...

This work presents a method of screening of alkanophenoxy carboxylic (2,4-D, 2,4,5-T, MCPA, MCPP) and phenolic (dinoterb, dinoseb, pentachlorophenol) herbicides in water. The successive steps of the method, i.e. liquid-liquid extraction with ethyl acetate and methyl-tert-butyl ether and solid phase extraction using C18-modified silica gel and styrenedivinylbenzene copolymer-packed cartridges as...

A rapid simulated distillation method is described for analysis of petroleum fractions boiling within the range of ASTM D2887 [1]. The method employs an Agilent 6890N gas chromatograph (GC) equipped with a split/splitless inlet, flame ionization detector (FID), oven insert, and 3-meter 180-μm id capillary column. A SIMDIS software package is partially integrated into the GC ChemStation for data...

The chemical composition of oregano essential oil of different origin extracted from oregano plants grown in south-eastern Poland was analysed using the gas chromatography mass spectrometry (GC-MS) and gas chromatography flame ionization detector (GC-FID). The dominant compound was sabinene; its percentage proportion ranged from 10.85% to 25.46%, depending on the ecotype studied. Moreover, the ...

The volatile oils from leaves of Michelia champaca L. collected bimonthly during one year (four times on the fifteenth day of January, March, May, July, September, and November 2004) were subjected to GC/FID and GC-MS analysis, from which thirteen components were identified. Additionally, part of the oil obtained from January collection was subjected to fractionation over silica gel soaked with...

Using gas chromatography with flame ionization detection and electroantennographic detection in parallel (GC-FID/EAD), the active constituents of the sex attractant of male dung beetles of Kheper bonellii were located in the gas chromatogram of an extract of the secretion. These constituents were identified as propanoic acid, butanoic acid, indole, 3-methylindole (skatole) and methyl cis-cascar...