Aroma recovery as determined by solid phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS) was compared in coffees resulting from conventional grinding processes, and from wet grinding with cold and hot water. Freshly roasted coffee as well as old, completely degassed coffee was ground in order to estimate the relationship of internal carbon dioxide pressure in freshly roaste...

High energy ball mills are used to grind powder material down to a particle size below one micron. Up to now, the detailed physical mechanisms of the grinding process inside the mill have not been fully understood. Hence, the design of these mills as well as their process parameters is based on empirical results. The ball mill has been simulated by discrete event simulation (DES) using typical ...

pure azo schiff bases were readily and conveniently accessible in high yields by mixing of the reagents either as aqueous slurry, or by grinding at room temperature. this method, unlike a classical method, needs neither harsh conditions nor organic solvents. the satisfactory results were obtained with excellent yields, short reaction time, and operational simplicity in the experimental procedur...

Forces generated during precision wafer grinding are small and present challenges for accurate and reliable process monitoring. In this work, these challenges are met by incorporating noncontact displacement sensors into an aerostatic spindle that is calibrated to measure grinding forces from the relative motion between the spindle rotor and stator. This arrangement allows the calculation of gr...

The mechanochemical preparation of highly functionalized 3,5-disubstituted hydantoins was investigated in the presence of various poly(ethylene) glycols (PEGs), as safe grinding assisting agents (liquid-assisted grinding, LAG). A comparative study under dry-grinding conditions was also performed. The results showed that the cyclization reaction was influenced by the amount of the PEG grinding a...

The direct and indirect methods in solvent media and grinding method in a solvent-free media were used to prepare the MCM-41/ZnO and MCM-48/ZnO photocatalysts. The X-ray diffraction (XRD) patterns showed that zinc oxide nanoparticles were put into MCM-41 and MCM-48 substrates and there were ZnO crystallites as secondary phase in the extra framework of mesoporous materials. The decrease of surfa...

This paper presents an application of the Taguchi method parameter design to optimize the surface roughness, tool wear and cutting force by hard turning process. The Taguchi parameter design method is an efficient method in which response variable can be optimized, given various controls and using fewer experimental runs. Hard turning is the latest trend in all manufacturing industries and it i...

This study characterized exposure for dust-producing construction tasks. Eight common construction tasks were evaluated for quartz and respirable dust exposure by collecting 113 personal task period samples for cleanup; demolition with handheld tools; concrete cutting; concrete mixing; tuck-point grinding; surface grinding; sacking and patching concrete; and concrete floor sanding using both ti...