نتایج جستجو برای: 1hnmr

تعداد نتایج: 557  

Journal: :Heliyon 2023

The activity of alginic acid as a cytotoxic agent was improved by structure modification using 4-aminophenol (4-AP) through condensation and polymerization processes. Then, silver nanoparticles were employed doping to further enhance the modified polymer. prepared materials characterized FT-IR, 1HNMR, UV spectroscopy, X-ray diffraction, electron microscopy, thermal behavior all synthesized inte...

Journal: :iranian chemical communication 0
abhijeet somwanshi research centre and post graduate department of chemistry, padmashrivikhepatil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribaiphule pune university, pune) yashwant bhaskar pandit applied chemistry division, diat-drdo, girinagar, pune. 411025.(ms) india. akash gholap research centre and post graduate department of chemistry, padmashrivikhe patil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribai phule pune university, pune) rushikesh ghogare research centre and post graduate department of chemistry, padmashri vikhe patil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribai phule pune university, pune) shivaji pandit post graduate and research centre, department of chemistry, padmashri vikhe patil college of arts, science and commerce pravaranagar, (loni kd) tal. rahata. dist. ahmednagar 413713 (ms) india.

an efficient one pot multi component synthesis of 1, 4-polyhydroquinoline derivatives through unsymmetrical hantzsch reaction using lanthanum chloride heptahydrate (lacl3.7h2o) from an aromatic aldehyde, ethyl acetoacetate, dimedone and ammonium acetate as a nitrogen precursor in ethanol at room temperature is described. in the present work we report lanthanum chloride heptahydrate remarkably n...

ژورنال: :پژوهش های کاربردی در شیمی 0
کعبه رهنمای لاکمه سری دانشجوی دکترای شیمی آلی، دانشکده علوم پایه، واحد مشهد، دانشگاه آزاد اسلامی، مشهد، ایران سعید تقوایی گنجه علی استاد شیمی آلی، دانشکده شیمی، واحد تهران شمال، دانشگاه آزاد اسلامی، تهران، ایران رضا زادمرد دانشیار شیمی آلی، پژوهشگاه شیمی و مهندسی شیمی ایران، تهران، ایران مینا روشنی دانشیار شیمی آلی، دانشکده علوم پایه، واحد مشهد، دانشگاه آزاد اسلامی، مشهد، ایران

در این پژوهش مشتق تترا آزوکالیکس [4] آرن بر پایه 2 و 6- دی آمینو پیریدین به وسیله واکنش کوپلینگ آزو میان نمک تترادیازونیوم کالیکس [4] آرن و 2 و 6- دی آمینو پیریدین سنتز شده است. شناسایی ترکیب به دست آمده به وسیله روش های طیف سنجی (فروسرخ، فرابنفش، 1hnmr ، 13cnmr و جرمی) صورت گرفت. ویژگی ضد باکتری با استفاده از آزمون رقیق سازی محیط کشت (broth macrodilution) انجام شد. این بررسی روی چهار سویه استا...

2011
Liming Xue Yin Wang Lei Liu Lu Zhao Ting Han Qiaoyan Zhang Luping Qin

A metabonomics method using (1)H nuclear magnetic resonance spectroscopy ((1)HNMR) was applied to obtain a systematic view of the development and progression of postmenopausal osteoporosis. Using partial least squares discriminant analysis (PLS-DA), 26 and 34 characteristic resonances were found respectively in urine and plasma of ovariectomized rats (Variable importance, VIP value ≥1.0), and t...

2017
Samir Dou Nathalie Villa-Vialaneix Laurence Liaubet Yvon Billon Mario Giorgi Hélène Gilbert Jean-Luc Gourdine Juliette Riquet David Renaudeau

The negative impact of heat stress (HS) on the production performances in pig faming is of particular concern. Novel diagnostic methods are needed to predict the robustness of pigs to HS. Our study aimed to assess the reliability of blood metabolome to predict the sensitivity to chronic HS of 10 F1 (Large White × Creole) sire families (SF) reared in temperate (TEMP) and in tropical (TROP) regio...

2016
Shirin Parvaz Sedigheh Sadeghi Mehri Azadi Maryam Mohammadi Mohammad Arjmand Farideh Vahabi Somye Sadeghzadeh Zahra Zamani

Malaria is responsible for estimated 584,000 deaths in 2013. Researchers are working on new drugs and medicinal herbs due to drug resistance that is a major problem facing them; the search is on for new medicinal herbs. Cinnamon is the bark of a tree with reported antiparasitic effects. Metabonomics is the simultaneous study of all the metabolites in biological fluids, cells, and tissues detect...

2018
Kaili Wang Mengjiao Qi Chunjing Guo Yueming Yu Bingjie Wang Lei Fang Mengna Liu Zhen Wang Xinxin Fan Daquan Chen

In this work, novel mitochondrial and CD44 receptor dual-targeting redox-sensitive multifunctional nanoparticles (micelles) based on oligomeric hyaluronic acid (oHA) were proposed. The amphiphilic nanocarrier was prepared by (5-carboxypentyl)triphenylphosphonium bromide (TPP), oligomeric hyaluronic acid (oHA), disulfide bond, and curcumin (Cur), named as TPP-oHA-S-S-Cur. The TPP targeted the mi...

2015
Hlamulo R. Makelane Oluwakemi Tovide Christopher E. Sunday Tesfaye Waryo Emmanuel I. Iwuoha

A novel dendritic star-copolymer, generation 3 poly(propylene thiophenoimine) (G3PPT)-co-poly(3-hexylthiophene) (P3HT) star co-polymer on gold electrode (i.e., Au|G3PPT-co-P3HT) was used as a sensor system for the determination of phenanthrene (PHE). The G3PPT-co-P3HT star co-polymer was synthesized via in situ electrochemical co-polymerization of generation 3 poly (propylene thiophenoimine) an...

2016
Daniel Admasu Desam Nagarjuna Reddy Kebede Nigussie Mekonnen

The rapid and continuous progress in trace analysis of metals is associated with development of several new techniques such as spectrophotometry. Thiosemicarbazones have been used as chromogenic reagents in spectrophotometric determination of metals. In this study the synthesis and characterization of pyridoxal thiosemicarbazone (PDT) and 2-acetyl pyridine thiosemicarbazone (2-APT) using IR, MS...

2001
D. ENETTE LARSON-MEYER BRADLEY R. NEWCOMER GARY R. HUNTER

Larson-Meyer, D. Enette, Bradley R. Newcomer, and Gary R. Hunter. Influence of endurance running and recovery diet on intramyocellular lipid content in women: a 1HNMR study. Am J Physiol Endocrinol Metab 282: E95–E106, 2002.—Using a randomly assigned crossover design, we evaluated the change in intramyocellular lipid stores (IMCL) from baseline after a 2-h treadmill run [67% of maximal oxygen u...

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