This guide sheet outlines a method for the analysis of cubic crystal forms, this being useful to you for interpreting the transmission diffraction pattern produced by scattering electrons off a thin film target of polycrystalline aluminium. The apparatus also contains samples with hexagonal structures. These are pyrolytic graphite targets, and are available both as single crystals and in polycr...

Advances made over the past decade in structure determination from powder diffraction data are reviewed with particular emphasis on algorithmic developments and the successes and limitations of the technique. While global optimization methods have been successful in the solution of molecular crystal structures, new methods are required to make the solution of inorganic crystal structures more r...

in this paper the reflection coefficient of electromagnetic wave incidence on the walls of the buildings and obstacles that occurs in mobile communication path was modified by solving the riccati nonlinear equations. for this purpose, the building walls are assumed inhomogeneous layers where their permittivity changes as function of the wall thickness. using this reflection coefficient, a new p...

X-ray, neutron and electron diffraction methods are widely used for the investigation of crystals. Each of these techniques has their own advantages in terms of element sensitivity, sample size requirements etc. and are chosen accordingly for structure determinations. A less obvious difference lies in the spatial resolution of these diffraction techniques. Here, we show that electron diffractio...

The floating-zone method with different growth ambiences has been used to selectively obtain hexagonal or orthorhombic DyMnO(3) single crystals. The crystals were characterized by x-ray powder diffraction of ground specimens and a structure refinement as well as electron diffraction. We report magnetic susceptibility, magnetization and specific heat studies of this multiferroic compound in both...

We present a detailed study of magnetism in LuFe(2)O(4), combining magnetization measurements with neutron and soft x-ray diffraction. The magnetic phase diagram in the vicinity of T(N) involves a metamagnetic transition separating an antiferro- and a ferrimagnetic phase. For both phases the spin structure is refined by neutron diffraction. Observed diffuse magnetic scattering far above T(N) is...

This paper shows a simple procedure for the quantification of industrial and laboratory samples of Ammonium Sulphate-Nitrate fertilizers (ASN) based on a Rietveld fit from X-ray powder diffraction profiles. The Rietveld fit is performed by means of the structural models of the double salts 2NH4NO3·(NH4)2SO4 and 3NH4NO3·(NH4)2SO4, previously reported by the authors. The proposed method demonstra...