a simple, rapid and sensitive solvent assisted-dispersive solid phase extraction method was developed for the extraction of iron(ii) prior to its spectrophotometric determination. the fe(ii) reacted with 2,4,6-tris(2-pyridyl)-1,3,5-triazine, neutralized with sodium dodecyl sulfate and extracted onto the fine particles of benzophenone which were formed upon rapid injection of a mixture of benzop...

a solid phase extraction sorbent based on polyaniline/graphene nanocomposite is presented. the structure and morphology of synthesized nanocomposite were investigated by fourier transform infrared spectroscopy, field emission scanning electron microscopy, x-ray diffraction and thermal gravimetric analysis. the dispersive solid phase extraction was employed to the isolation and preconcentration ...

Phthalate esters are endocrine disrupters or mutagens. They are widely used as plasticizers and can be usually found in environmental samples, such as food, soil and polluted air. However, it is difficult to directly determine phthalate esters owing to their relatively low concentration and complex matrices. Therefore, preconcentration and separation have become increasingly important. In recen...

A solid phase extraction sorbent based on polyaniline/graphene nanocomposite is presented. The structure and morphology of synthesized nanocomposite were investigated by Fourier transform infrared spectroscopy, field emission scanning electron microscopy, X-ray diffraction and thermal gravimetric analysis. The dispersive solid phase extraction was employed to the isolation and preconcentration ...

Recently, the solid phase extraction technology has received considerable attention considering serious environmental problems and much more contaminants present in the samples at trace level that is different to be analyzed. During the whole process of analyzing sample, the preconcentration of sample is the most complicated and significant step, which typically spend much time, affecting the a...

a chelating resin is prepared by condensation polymerization of aniline with formaldehyde andcharacterized by ft-ir, elemental analysis and studied for the preconcentration and determination of traceplatinum ion from environmental water sample using inductively coupled plasma-atomic emission spectroscopy(icp-aes). the optimum ph value for sorption of the metal ions was 5. the maximum adsorption...

styrene is an important constituent of widely used organic solvents in industries for production of various synthetic materials. the use of solid-phase extraction (spe) has grown and is a fertile technique of sample preparation as it provides better results than those produced by liquidliquid extraction. in this study, spe has been optimized, regarding sample ph, sample concentration, sample fl...

Abbreviations: AIBN, 2,20-azo-bis-isobutyronitrile; ASE, Accelerated solvent extraction; CAR, Carboxen; DAD, Diode-array detector; DI-SPME, Direct-immersion solid-phase extraction; DSPE, Dispersive solid-phase extraction; EGDMA, Ethylene glycol dimethacrylate; ESE, Enhanced solvent extraction; ESI, Electrospray ionization; FD, Fluorescence detection; FLD, Fluorimetric detection; GC, Gas chromat...

a simple and sensitive method has been developed for the preconcentration and determination of trace level of co(ii) using uv-vis spectrophotometry. β-cyclodextrin polymer modified with 1-(2-pyridylazo)-2-naphthol (pan) is used for the preconcentration of co(ii) from samples at ph 8.5. the polymer is synthesized and characterized using elemental analysis, ft-ir and sem analysis. the factors aff...