incorporation of copper species into silica matrix was performed by the sol-gel method. copper ions and copper particles were doped using two different copper sources; cu(no3)2.3h2o and copper particles chemically synthesized.the particles of copper metallic, cuprous and cupric oxide were prepared and the synthesis and characterizations of copper species were compared together. on the other han...

high purity lead titanate nanopowders in tetragonal form have been successfully prepared bycitric acid gel method using lead nitrate and tetra-n-butyl titanate as pb and ti sourcesrespectively and citric acid as complexing reagent. the precursors were calcined at varioustemperatures ranging from 450 °c to 600 °c for 2 h. fourier transform infraredspectroscopy (ft-ir), x-ray diffraction (xrd) an...

cobalt oxide (co3o4) nanorods were prepared by a simple co-precipitation method using ethanol solution of cobalt nitrate as precursor and cetyl trimethylammonium bromide (ctab) as surfactant. morphological properties of the nanoparticles were characterized. xrd measurement exhibited the structure of co3o4 nanocrystals for annealed samples. the sem images revealed that the particles changed from...

stoichiometric tetragonal bal-xsrxtio3 (x = 0.23) nanopowders were prepared by stearic acid gel(sag) method using barium stearate, strontium stearate, tetrabutyl titanate as ba, sr, ti sourcesand stearic acid as complexing reagent. thermal analysis including differential thermogravimetric(dtg) and tg, fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd) andtransmission electr...

sol–gel chemistry is an efficient tool to control the morphology and reactivity of solids. drying is the crucial step due to the capillary forces exerted during the classic ambient drying process, which induces the collapse of the wet gel porosity. the use of n, n-dimethylformamide (dmf), a newly found dcca were found to be effective in the sol–gel synthesis of crack-free silica gel monolith fr...

in this research, the thin films of n-s doped titanium dioxide (tio2) were successfully prepared by simple sol-gel method in the presence of tetrabutylorthotitanate as a starting reagent. furthermore, titanium dioxide (tio2) was functionalized with thiourea. furthermore, n-s doped titanium dioxides (nsto) were fixed on glass balls by glass balls fixed-bed reactor system. besides, the effect of ...

In this research, the thin films of N-S doped titanium dioxide (TiO2) were successfully prepared by simple sol-gel method in the presence of tetrabutylorthotitanate as a starting reagent. Furthermore, titanium dioxide (TiO2) was functionalized with thiourea. Furthermore, N-S doped titanium dioxides (NSTO) were fixed on glass balls by glass balls fixed-bed reactor system. Besides, the effect of ...