a quantitative analysis method for fudosteine in human serum by high-performance liquid chromatography-electrospray ionization tandem mass spectrometry (hplc-esi/ms/ms) was established, which shows high sensitivity and selectivity. the mobile phase composition was 75% 20 mm acetic acid and 25% acetonitril, which was pumped at a flow rate of 0.40 ml/min. the overall chromatographic run time was ...

the chemical components in the decoctions of chinese herbal medicines are not always the same as those in the crude herbs because of the insolubility or instability of some compounds. in this work, a high-performance liquid chromatography (hplc) coupled with electrospray ionization (esi) tandem mass spectrometry method was developed to explore dynamic variation patterns of aconitum alkaloids in...

high performance liquid chromatography (hplc) with diode array detection (dad) and electrospray ionization tandem mass spectrometry (esi/ms/ms) was used to analyze the main components in the methanol extract of fructus aurantii (fa) and the metabolites in rat biological samples after oral administration of the methanol extract of fa. there were 31 constituents identified in the extract of fa in...

the aim of this study was to determine the monthly dtr mass load of amphetamine-type compounds in poland as well as an investigation of cyclical behaviour by using time series analysis and especially trends analysis.amphetamine, methamphetamine and mdma (ecstasy) were detected in wastewater samples collected from the main wastewater treatment plant in the city of poznan using liquid chromatogra...