نتایج جستجو برای: Hantzsch Reaction

تعداد نتایج: 412554  

Journal: :Advanced pharmaceutical bulletin 2011
Javid Shahbazi Mojarrad Zahra Zamani Hossein Nazemiyeh Saeed Ghasemi Davoud Asgari

INTRODUCTION We report the synthesis of novel 1,4-dihydropyridine derivatives containing biphenyl-2'-tetrazole moieties. We hypothesized that merging the key structural elements present in an AT1 receptor antagonist with key structural elements in 1,4-dihydropyridine calcium channel blockers would yield novel analogs with potential dual activity for both receptors. This strategy led to the desi...

2013
Mark C Bagley Vincenzo Fusillo Robert L Jenkins M Caterina Lubinu Christopher Mason

The Bohlmann-Rahtz pyridine synthesis and the Hantzsch dihydropyridine synthesis can be carried out in a microwave flow reactor or using a conductive heating flow platform for the continuous processing of material. In the Bohlmann-Rahtz reaction, the use of a Brønsted acid catalyst allows Michael addition and cyclodehydration to be carried out in a single step without isolation of intermediates...

2012
Cosmas O. Okoro Tasneem Siddiquee

This article describes one-pot synthesis of new fluorinated hexahydroquinoline derivatives via unsymmetric Hantzsch reaction involving 5-trifluoromethyl-1,3cyclohexanedione, aldehydes, acetoacetate ester, and ammonium acetate in trifluoroethanol (TFE). The reaction is simple and rapid with high yield.

Journal: :iranian chemical communication 0
abhijeet somwanshi research centre and post graduate department of chemistry, padmashrivikhepatil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribaiphule pune university, pune) yashwant bhaskar pandit applied chemistry division, diat-drdo, girinagar, pune. 411025.(ms) india. akash gholap research centre and post graduate department of chemistry, padmashrivikhe patil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribai phule pune university, pune) rushikesh ghogare research centre and post graduate department of chemistry, padmashri vikhe patil college of arts, science and commerce pravaranagar at./po. lonikd. tal.rahata. dist. ahmednagar. 413713. (ms). india. (affiliated to savitribai phule pune university, pune) shivaji pandit post graduate and research centre, department of chemistry, padmashri vikhe patil college of arts, science and commerce pravaranagar, (loni kd) tal. rahata. dist. ahmednagar 413713 (ms) india.

an efficient one pot multi component synthesis of 1, 4-polyhydroquinoline derivatives through unsymmetrical hantzsch reaction using lanthanum chloride heptahydrate (lacl3.7h2o) from an aromatic aldehyde, ethyl acetoacetate, dimedone and ammonium acetate as a nitrogen precursor in ethanol at room temperature is described. in the present work we report lanthanum chloride heptahydrate remarkably n...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2002
Tohru Saitoh Keita Taguchi Masataka Hiraide

The reaction of formaldehyde with β-diketones (Hantzsch reaction) has been often employed for derivatizing formaldehyde to the fluorescent compounds.1,2 Among βdiketones, 5,5-dimethyl-1,3-cyclohexanedione (dimedone, Fig. 1) seems to be the most promising because of the strong fluorescence intensity and stability of the formed compound. Recently, we developed a method for concentrating trace hyd...

Journal: :Molecules 2007
Mirela Filipan-Litvić Mladen Litvić Ivica Cepanec Vladimir Vinković

Hantzsch condensation of two equivalents of methyl-3-aminocrotonate with (m- and p)-methoxybenzaldehyde afforded the expected products 2,6-dimethyl-3,5-dimethoxycarbonyl-4-(m-methoxyphenyl)-1,4-dihydropyridine and 2,6-dimethyl-3,5-dimethoxycarbonyl-4-(p-methoxyphenyl)-1,4-dihydropyridine, whereas o-methoxy-benzaldehyde produced mainly 1-amino-2-methoxycarbonyl-3,5-bis(o-methoxy-phenyl)-4-oxa-cy...

Journal: :iranian journal of catalysis 2011
farhad shirini seyyed vahid atghia meysam alipour khoshdel

an efficient synthesis of polyhydroquinoline derivatives was reported via four-component coupling reactions of aldehydes, 1,3-dicarbonyl ketones (dimedone or 1,3-cyclohexanedione), ethyl acetoacetate or methyl acetoacetate and ammonium acetate in the presence of a catalytic amount of nanocrystalline tio2 under solvent free conditions. the reported method is mild, rapid and has the advantages su...

Journal: :Chemical communications 2011
Nadiya Koukabi Eskandar Kolvari Ardeshir Khazaei Mohammad Ali Zolfigol Behzad Shirmardi-Shaghasemi Hamid Reza Khavasi

A magnetic nanoparticle catalyst was readily prepared from inexpensive starting materials which catalyzed the Hantzsch reaction. High catalytic activity and ease of recovery from the reaction mixture using an external magnet, and several reuse times without significant losses in performance are additional eco-friendly attributes of this catalytic system.

Journal: :Chemical communications 2011
Ming Zhang Hongwei Yang Yan Zhang Chengjian Zhu Wei Li Yixiang Cheng Hongwen Hu

The direct reductive amination of aromatic aldehydes has been achieved with excellent isolated yields (89-96%) using readily accessible Ph(3)PAuCl/AgOTf catalyst along with ethyl Hantzsch ester as hydrogen source under mild reaction conditions.

An efficient one pot multi component synthesis of 1, 4-Polyhydroquinoline derivatives through unsymmetrical Hantzsch reaction using lanthanum chloride heptahydrate (LaCl3.7H2O) from an aromatic aldehyde, ethyl acetoacetate, dimedone and ammonium acetate as a nitrogen precursor in ethanol at room temperature is described. In the present work we report lanthanum chloride heptahydrate remarkably n...

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