نتایج جستجو برای: Nickel determination

تعداد نتایج: 284032  

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2003
farzaneh shemirani mahdi zamani mohammad reza jamali

a column of alumina modified with sodium dodecyl sulfate (sds) and dimethylglyoxime (dmg) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (faas) determinations. under optimized conditions (ph=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. the nickel collected on the column was eluted with 5 ml of 1 m nitric acid. ...

Journal: :journal of the iranian chemical research 0
jahan b. ghasemi chemistry department, faculty of sciences, k.n. toosi university of technology, tehran, iran samira kariminia chemistry department, faculty of sciences, razi university, kermanshah, iran

a partial least squares (pls) calibration model was developed for the simultaneous spectrophotometricdetermination of pb (ιι), cu (ιι) and ni (ιι) using xylenol orange as a chromogenic reagent. the parameterscontrolling behavior of the system were investigated and optimum conditions were selected. the calibrationgraphs were linear in the ranges of 0.0–9.091, 0.0–2.719 and 0.0–2.381 ppm for lead...

Journal: :Acta chimica Slovenica 2012
Reyhaneh Rahnama Zeynab Chamani Jojadeh Mohammad Reza Jamali

A new method of dispersive liquid-liquid microextraction (DLLME) combined with UV-Vis spectrophotometry was proposed for the determination of trace nickel using 2,2'-Furildioxime as chelating and spectrophotometric reagent. In the proposed approach chloroform and ethanol were used as extraction and dispersive solvents, respectively. Some factors influencing the extraction efficiency of nickel a...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2003
Qiufen Hu Guangyu Yang Zhangjie Huang Jiayuan Yin

A sensitive, selective and rapid method for the determination of nickel based on a rapid reaction of nickel(II) with 2-(2-quinolylazo)-5-diethylaminoaniline (QADEAA) has been developed. In the presence of pH = 6.0 ammonia-ammonium chloride buffer solution and sodium dodecyl sulfonate (SDS) medium, QADEAA reacts with nickel to form a violet complex having a molar ratio of 1:2 (nickel to QADEAA)....

2015
B. Ranganath Saleem Basha M. R. Jayapal Venkata Ramana

Esomeprazole is a new chromogenic reagent used for the determination of nickel (II) by direct spectrophotometric method. Esomeprazole forms a greenish yellow colouredcomplex with nickel (II) at pH 5. The method obeys Beer’s law over 0.139 – 1.394 μg mL -1 , Sandell’s sensitivity is 0.0029mg/cm 2 and molar absorptivity value (ε = 2.5 x 10 4 L mol -1 cm -1 ). The method is useful for determinatio...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2010
Sayed Zia Mohammadi Daryoush Afzali Yar Mohammad Baghelani

In the present work, a new ligandless-ultrasound-assisted emulsification microextraction (LL-USAEME) method was developed for preconcentration trace amounts of nickel as a prior step to its determination by flame atomic absorption spectrometry. Some factors influencing the extraction efficiency of nickel and its subsequent determination were studied and optimized, such as type and volume of the...

2005
Viorica COSMA

Taking into account the use of Nickel brasses in industry a great number of methods for the determination of Ni have been reported. More, theoretical predictions of free Cd increasing with decreasing salinity have been confirmed using cadmium selective electrodes. The method under proposal, for the determination of nickel ions in brass alloys consists of the following steps: Cu masking with sod...

Journal: :Annals of clinical and laboratory science 1977
E S Baginski S S Marie E Epstein B Zak

A simple determination of 5'-Nucleotidase in blood serum without deproteinization is described. The enzyme activity is distinguished from that of a nonspecific alkaline phosphatase by nickel inhibition and the inorganic phosphate released from adenosine monophosphate used as substrate is determined by a method previously described. Additional studies include the determination of optimal conditi...

2011
María Carmen Yebra-Biurrun Jesús Manuel Castro-Romero

A simple on-line sonodigestion system was successfully used for breakdown organic nickel complexes in environmental waters acidified with diluted nitric acid prior to flow injection total dissolved nickel preconcentration in a microcolumn containing a chelating resin (Chelite Che with iminodiacetic acid groups) and determination by flame atomic absorption spectrometry. For the determination of ...

Journal: :Journal of the American Chemical Society 1894

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