نتایج جستجو برای: Process Parameters, Sol-Gel Methods
تعداد نتایج: 3427084 فیلتر نتایج به سال:
as we know sol-gel is one of the most important techniques for thin film preparation. in this paper, high transmission silica thin films have been prepared by dip-coating process from a new silicon-alkoxide solution. the prepared sol was stable for 45 days which is very important to characterize the coating process. the optical properties as a function of aging time, withdrawal rate, and heat t...
In this study, TiB2 particles were synthesized by sol-gel method in nanometer size. First, the sol was prepared in a four-component system of alkoxide -boron carbide -water-alcohol based on the sol-gel chemical process under acidic conditions at pH = 5. Titanium tetra-isopropoxide and boron carbide were used as raw materials. After hydrolysis and gel formation followed by heat treatment, TiB2 n...
We report on the fabrication and characterization of thick UV-patternable hybrid sol-gel films by spin coating using a modified sol-gel process. Thick coating of 25 microns with crack-free surface can be produced by one spin coating step. Thick layers of more than 100 μm can be obtained with a multi-coating process. Characterization using different techniques including optical microscope and at...
the photocatalytic coatings were prepared via incorporating the modified titania nanoparticles into epoxy-based inorganic-organic hybrid coatings. titania nanoparticles were first synthesized from tetra-n-butyl titanate using sol-gel methods by two different calcination treatments, i.e., in mild condition (80°c) and 500°c. the formed anatase nanoparticles were further modified as titania-silica...
The sol-gel process has emerged as an effective route for the fabrication of optical waveguides and guided wave devices and circuits. In particular, it is possible to incorporate active dopants like neodymium, erbium, and cesium for integrated optical active devices and circuits. In this paper, a review of recent research on active devices and circuits based on sol-gel process is made. Specific...
As we know sol-gel is one of the most important techniques for thin film preparation. In this paper, high transmission silica thin films have been prepared by dip-coating process from a new silicon-alkoxide solution. The prepared sol was stable for 45 days which is very important to characterize the coating process. The optical properties as a function of aging time, withdrawal rate, and he...
The sol-gel method is a simple and facile wet chemical process for fabricating advanced materials with high homogeneity, high purity, and excellent chemical reactivity at a relatively low temperature. By adjusting the processing parameters, the sol-gel technique can be used to prepare hollow sphere and 1D structural materials that exhibit a wide application in the fields of catalyst, drug or ge...
nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize zno/cuo nanocomposi...
This paper describes the synthesis of Pb(Zr0.95Ti0.05)O3 powder by sol gel and solid state methods. PZT powders were fabricated by solid-state reaction process using metal oxides and in sol gel method salts and organic compounds were employed. The powders were calcined at 700 and 950 oC in sol gel and solid state methods, respectively. The synthesized powders were analyzed by FTIR and XRD. Th...
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