nowadays, it has demonstrated that viruses can be transmitted by water and foods. therefore, it causes the research to develop for detecting different viruses in water and foods. among foods, milk can transfer potentially pathogenic viruses. on the other hand, to achieve every method for recovery and extraction of viruses in raw milk it needs to know about impact of milk components on viruses. ...

A technique for the selective measurement of diffusive gradients in thin-films (DGT) for free Cu2+ ions was developed using a 0.030 M solution of polyvinyl alcohol (PVA) as the liquid binding phase with the liquid-type DGT devices (PVA DGT). The PVA DGT had a substantial binding capacity at pH 5.6 - 8.6 and concentrations of competitive Na+ up to 0.7 M. The measurements of PVA DGT and cupric io...

OBJECTIVES The purpose of this research was to develop a determination method for nitromethane (NM) in workplace air for risk assessment. METHODS A suitable sampler and appropriate desorption condition were selected by a recovery test in which a spiked sampler was used. The characteristics of the proposed method, such as recovery, detection limit, and reproducibility, and the storage stabilit...

To determine cypermethrin and permethrin in agricultural products, a competitive enzyme-linked immunosorbent assay (ELISA) method was employed. The matrix interferences were minimized by direct dilution of the extracts. No further cleanup was needed. A minimum matrix effect with a 1:10 dilution of white wine for cypermethrin and a 1:200 dilution of red and white wines, fruits, and vegetables fo...

a fast and simple modified quechers (quick, easy, cheap, rugged and safe) extraction method based on spiked calibration curves and direct sample introduction was developed for determination of benzo[a]pyrene (bap) in bread by gas chromatography-mass spectrometry single quadrupole selected ion monitoring (gc/ms-sq-sim). sample preparation includes extraction of bap into acetone followed by clean...

The assessment of the recovery factor with the analyte concentration in meat samples has been studied for the determination of organochlorine and organophosphorus pesticides in meat by gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS). For that purpose, recent IUPAC recommendations, which distinguishes between two terms, recovery factor and apparent recovery, have been followed....

A method for the determination of six organochlorine pesticides in human serum is proposed. Serum samples containing in vitro spiked pesticides (alpha-HCH, beta-HCH, gamma-HCH, p,p'-DDE, o,p'-DDT, and p,p'-DDT) were used to evaluate the method. The method involved pesticide extraction from a serum-silica suspension with n-hexane-acetone (9:1), extract purification using alumina-column chromatog...