Double-walled TiO2 nanotubes with porous wall morphologies are fabricated by anodization under ultraviolet (UV) irradiation. TiO2 formed by anodization of Ti is activated to generate electrons and holes by UV and the anodization process is influenced by the photo-generated charges. As a consequence, morphologies of the fabricated TiO2 nanotubes can be adjusted by controlling the UV illumination...

TiO2/WOx nanotubes have unique photo-energy retention properties that have gathered scientific interest. Herein, we report the synthesis, morphological characterization, and the electrochemical characterization of TiO2/WOx nanotubes compared with pure TiO2 nanotubes, prepared by anodization technique. Significant structural differences were not observed in TiO2/WOx nanotubes as observed by usin...

Alumina (Al2O3) decorated anatase TiO2 nanotubes with ordered mesoporous pore walls (Al2O3/meso-TiO2 nanotubes) are successfully synthesized through vacuum pressure induction technology, and then combined with the thermal decomposition of a mesoporous TiO2 sol precursor, inside the cylindrical nanochannels of an anodic aluminium oxide (AAO) template. The decorated Al2O3 was formed by in situ de...

This study compared the responses of Pd-functionalized and pristine titanate (TiO2) nanotube arrays to ethanol with those to acetone to determine the effects of functionalization of TiO2 nanotubes with Pd nanoparticles on the sensitivity and selectivity. The responses of pristine and Pd-functionalized TiO2 nanotube arrays to ethanol gas at 200 °C were ~2877% and ~21,253%, respectively. On the o...

Regularly spaced TiO2 nanotubes were prepared by anodizing a titanium substrate in triethylene glycol electrolyte at elevated temperature. In comparison to conventional TiO2 nanotubes, spaced nanotubes possess an adjustable spacing between the individual nanotubes; this allows for controlled buildup of a hierarchical nanoparticle-on-nanotube structure. Here, we use this principle for layer-by-l...

Using magnetron sputtering and heat treatment, Ag@TiO2 nanotubes are prepared. The effects of heat-treatment temperature and heating time on the evolution of Ag nanofilms on the surface of TiO2 nanotubes and microstructure of Ag nanofilms are investigated by X-ray diffraction, field emission scanning electron microscopy, and transmission electron microscopy. Ag atoms migrate mainly on the outmo...

In this study, we used the electrochemical anodization to prepare TiO2 nanotube arrays and applied them on the photoelectrode of dye-sensitized solar cells. In the field emission scanning electron microscopy analysis, the lengths of TiO2 nanotube arrays prepared by electrochemical anodization can be obtained with approximately 10 to 30 μm. After titanium tetrachloride (TiCl4) treatment, the wal...

TiO2 nanostructures, including nanowires, highly ordered nanotube arrays, and single crystalline nanoplates, were obtained from electrochemically anodized Ti foil in a fluorine-containing ethylene glycol electrolyte. The TiO2 nanowires, formed by the electric field induced chemical splitting of TiO2 nanotubes by fluoride ions during a lengthy anodization can be isolated from the nanotube arrays...

to improve the photo-catalytic degradation of salicylic acid, we reported the fabrication of ordered tio2 nanotube arrays by a simple and effective two-step anodization method and then these tio2 nanotubes treated in a methanol solution under uv light irradiation. the tio2 nanotubes prepared in the two-step anodization process showed better photo-catalytic activity than tio2 nanotubes prepared ...

One-dimensional nanotube systems with high surface-to-volume ratios possess unique properties and are thus utilized in various applications. In this study, self-organized TiO2 nanotubes were prepared by anodization of a Ti foil in glycerol containing 5 wt% ammonium fluoride (NH4F) and 6 wt% ethylene glycol (EG). The surface morphology, average inner diameter, and average length of the nanotubes...