a very simple, rapid and sensitive dispersive liquid-liquid microextraction (dllme) followed by gas chromatography and flame ionization detection (gc-fid) was developed for the determination of phenol and carvacrol in honey samples. a mixture of 100 µl dichloromethane (extraction solvent) and 0.5 ml acetonitrile (disperser solvent) was rapidly injected into sample solution. thereby a cloudy sol...

Aroma composition is critical to the quality of rice wine. In order clarify effect different koji on aroma components The Yuanyang was selected as raw material, and three kinds wine were added during fermentation. samples fermented at 31 °C for nine days qualitatively quantitatively analyzed by headspace solid-phase microextraction gas chromatography-mass spectrometry (HS-SPME-GC-MS). results s...

BACKGROUND We sought to develop a technique with the potential to partly replace current methods of analysis based on blood draws. To achieve this goal, we developed an in vivo microextraction technique that is faster than conventional methods, interferes minimally with the investigated system, minimizes errors associated with sample preparation, and limits exposure to hazardous biological samp...

Substances classified as unknown or variable composition, complex reaction products biological origin (UVCB) present a challenge for environmental hazard and risk assessment. Here, we novel approach whole-substance bioconcentration testing applied to cedarwood oil—an essential oil composed of volatile, hydrophobic organic chemicals. The method yields whole-body elimination rate constants mixtur...