In normal Amount Total Error of recovery Method plasma added found (%) Spectrophotometric 079 0-5 1*28 -3-4 1*0 0.4 1*41 +2-5 -1*0 1.0 1*96 -4.0 -0-82 0-7 1-53 +1*4 -0*82 1*2 2*18 -1*7 Photoelectric 076 0 5 1F24 -4 0 -1-03 0-4 1*43 +1'2 -1-03 1.0 2*0 -3*0 -0'84 0 7 1*56 +2-8 -0*84 1*2 2*01 -2.5 Roe & Kuether (1943) -0-72 0 5 1-2 -4 0 -1.0 0.4 1*4 0.0 -1.0 1.0 1*96 -4*0 -0*88 0*7 1*6 +2-8 -0*88 ...

Benzyl 2-((E)-to yliminomethyl)penylcarbamat was prepared in good yield and characterized by the condensation reaction of benzyl 2-formylphenylcarbamate with ptoluenesulfonyl amine. The structure of the newly synthesized compound was determined using 1H, 13C-NMR, IR and ass s ectral data.

A new concept of nanoporous metal organic framework particles stabilising emulsions was investigated. The copper benzenetricarboxylate MOF particles adsorbed at the oil/water interface play an exceptional role in stabilising both oil-in-water and water-in-oil emulsions.

The hydrothermal reactions of [A-α-PW9O34](9-) with CuCl2·2H2O in the presence of ethanediamine (en) and acetate afforded a novel poly(polyoxotungstate) containing different lacunary fragments: monolacunary {α-PW11O39}, dilacunary {α-PW10O37}, trilacunary {B-α-PW9O34}, etc. In addition, a cockhorse-like nona-copper {Cu9} slab is incorporated. Magnetic investigation indicates overall antiferroma...

Correction for 'Highly photoluminescent copper carbene complexes based on prompt rather than delayed fluorescence' by Alexander S. Romanov et al., Chem. Commun., 2016, 52, 6379-6382.

In the title compound, [Al(CH(3))(C(23)H(15)F(10)N(3))], the Al(III) atom is coordinated in a distorted tetra-hedral geometry by three N atoms from the tridentate amine and by one C atom of the methyl substituent. Further, there is a short intra-molecular Al⋯F contact [2.5717 (11) Å], leading to an overall distorted trigonal-bipyramidal coordination environment around Al(III).

Kinetic resolution of 6-aryl-2,6-hexanediones was achieved with chiral secondary amine catalyzed intramolecular aldolization. The current kinetic resolution protocol enables the synthesis of both enantiomers of cyclohexenones with moderate to good enantioselectivity.