the aim of this research is to study ni2+ supported on hydroxyapatite-core-shell magnetic γ-fe2o3 nanoparticles (γ-fe2o3@hap-ni2+) as a green and recyclable catalyst for the biginelli reaction under solvent-free conditions. one-pot multi-component condensation of 1,3-dicarbonyl compounds, urea and aldehydes at 80 oc affords the corresponding compounds in high yields and in short reaction times ...

an improved, simple, and facile synthesis of 3,4-dihydropyrimidin-2(1h)-ones by employing three-component, one-pot condensation reaction of β-keto ester, aromatic aldehydes, and urea or n-methylurea using lacl3/clch2cooh as an inexpensive and green chemistry catalyst system under solvent-free conditions described. compared with the classicalbiginelli reaction conditions, this method has the adv...

background and purpose: the goal of this study is application of the proportional hazards model (ph) and accelerated failure time model (aft), with consideration weibull distribution, to determine the level of effectiveness of the factors affecting on the level of disease-free survival (dfs) of the patients with breast cancer. materials and methods: based on the retrospective descriptive studie...

the performance of many traffic control strategies depends on how much the traffic flow models are accurately calibrated. one of the most applicable traffic flow model in traffic control and management is lwr or metanet model. practically, key parameters in lwr model, including free flow speed and critical density, are parameterized using flow and speed measurements gathered by inductive loop d...

background and objectives: the quality of cakes made of wheat flour depends on the quantity and quality of its gluten proteins however, these proteins may have side effects for some people, including the patients with celiac, and the only way to cure this disease is to take a lifelong gluten-free diet. materials and methods: this research aims to produce gluten- free cake by using rice flour an...

oxidation of some benzoins to benziles is reported by using p-toluenesulfonic acid as aselective oxidation catalyst under solvent-free condition in high yield. the adjacent carbonylgroup is necessary for the oxidation of hydroxyl group in these compounds. the reaction iscarried out in a sand-bath at 100 °c with minimum by-products.

abstract introduction: medicinal plants belong to lamiaceae family are potential sources of new drugs to improve the treatment of diseases which its treatment is linked to anti-oxidative agents. in this paper, antioxidant potentials of some lamiaceae species have been evaluated by two methods. methods: phosphomolybdate assay for total antioxidant capacity and ferric reducing antioxidant potenti...

this work presents free vibration analysis of laminated rectangular plates with classical boundary conditions based on the classical plate theory (cpt). the first involves an s-fgm plate with different boundary conditions. then involves a two-layer plate in which an s-fgm layer is coated on a homogeneous substrate with classical boundary conditions, simply called an s-fgm-coated plate; the othe...

free vibration of simply supported circular cylindrical shell made of functionally graded material (fgm) under internal pressure was investigated. the effective material properties are assumed to vary continuously along the thickness direction according to a volume fraction power law distribution. first order shear deformation theory based on love's first approximation theory was utilized in th...

date juice was treated by cross- flow ultra-filtration with molecular weight cut-off (mwco) of 5 kda. optimized levels of feed brix, tmp and operation time were determined as 47.13, 82.11 psi and 30 min, respectively. under such conditions, 80.94% decolourisation and 97.78 % turbidity reduction were obtained while loss of glucose and fructose were estimated to be only 3.49% and 9.62%, respectiv...