A colorimetric method for detection and assay of mustard gas in urine after addition of thymolphthalein is reported. The detection limit was 80 ng/ml of llrine. Mustard gas could also be detected in urine after extraction with gas chromatography using FID detector. The detection limit was 10 ng/ml. In addition, thiodiglycol, a metabolite of mustard gas, could be converted to mustard with ...

[1] A rapid headspace method for the simultaneous laboratory determination of intentionally introduced hydrologic tracers, sulfur hexafluoride (SF6), trifluoromethyl sulfur pentafluoride (SF5CF3), Halon 1211 (CF2ClBr), and other halocarbons in water and gases is described. The high sensitivity of the procedure allows for introduction of minimal tracer mass (a few grams) into hydrologic systems ...

We describe the use of electron-capture gas chromatography or reversed-phase "high-performance" liquid chromatography for concurrent analysis for diazepam and nordiazepam in serum. In the gas-chromatographic analysis our use of a new chemically deactivated stationary liquid phase, SP 2250-DB (Supelco, Inc.), resulted in improved chromatographic sensitivity and peak symmetry for the two benzodia...

We tested for residual pesticide levels in dried vegetables in Seoul, Korea. A total of 100 samples of 13 different types of agricultural products were analyzed by a gas chromatography-nitrogen phosphate detector (GC-NPD), an electron capture detector (GC-μECD), a mass spectrometry detector (GC-MSD), and a high performance liquid chromatography-ultraviolet detector (HPLC-UV). We used multi-anal...

objective: the usage of pesticides has increased during the recent years. one the other hand, presence of harmful pesticides residue in rice and other food has caused a great concern among the consumers. therefore, it is important to develop some pragmatic procedures to increase the food safety along with the reduction in consumption of pesticide residues. methods: a gas chromatograph with elec...

A gas chromatographic method for the simultaneous analysis of halothane and nitrous oxide in operating theatre atmospheres has been developed and evaluated. The flame ionization detector is suitable for the quantitative analysis of halothane in concentrations approaching one part per million. The frequency-modulated electron capture detector is highly sensitive to nitrous oxide but we have foun...

The paper presents two methods for determination of phthalates in polymer materials. The methods compared were gas chromatography combined with the mass spectrometry (GC/MS) and gas chromatography with electron capture detector (GC/ECD). The GC/ECD technique was chosen for this comparison, because the ECD detector was one of few capable of detecting phthalates. In both cases the same procedure ...

in the present study, tenorite (cuo) nanoparticles have been assayed for their catalytic properties. the decontamination reaction of chloro ethyl ethyl sulfide (cees) as an surrogate of sulfur mustard simulant have been accomplished on the surface of cuo nps with different weight ratios at ambient temperature and monitored by gas chromatography equipped with flame ionization detector (gc-fid) a...

detected in these blank determinations that we were not certain whether it came from the Soluene or other sources. You may note that the blood of control rats which was analyzed with the use of Soluene did not contain detectable amounts of asbestos and zero fibers per gram was reported. We have since repeated this work (as yet unpublished) in an experiment in which asbestos was fed to rats and ...

In this study, the level of selected organophosphorus and organochlorine pesticide residues from water samples of Gilgle Gibe (I) hydroelectric dam reservoir and its potential tributaries, Jimma zone, Ethiopia, was determined by gas chromatography-electron capture detector (GC-ECD). Low density based dispersive liquid-liquid microextraction (LD-DLLME) using toluene (as extractant) and acetonitr...