The hydro-distilled essential oil from the fresh aerial part of Orchidantha vietnamica K. Larsen collected Lamdong-Vietnam was analyzed by GC-FID (Gas Chromatography-Flame Ionization Detection) and GC-MS Chromatography-Mass Spectroscopy) for first time. characterized presence volatile compounds type terpenoids, in which oxygenated monoterpenes (30.04 %) sesquiterpene hydrocarbons (37.32 are maj...

This paper describes four recent applications of analytical pyrolysis in environmental science and engineering. In all applications, samples were analyzed in order to provide information about the origin of organic matter or changes to an organic matrix. In the first application, pyrolysis-gas chromatography/mass spectrometry (GC/MS) and pyrolysis-GC/flame ionization detection (FID) were used t...

The Bordeaux grape variety is the most used in production of red juices. objective work was to evaluate carotenoids, flavonoids, vitamins C, E and B complex, total fatty acids, phytates, tannins, antioxidant capacity, phenolic compounds centesimal composition whole (W) defatted (D) seed flours oil (O). Total acids were evaluated by gas chromatography (flame ionization detector). Analysis comple...

Alkanolamines are anthropogenic compounds used extensively not only in the processing of sour natural gas but in other operations such as the petrochemical and fossil-fuel fired industries to reduce and prevent the emission of green house gases into the environment. Alkanolamines also find uses as corrosion inhibitors, emulsifying agents and in pharmaceutical formulations (Dobberpuhl and Johnso...

In this study, two methods are developed for the extraction of 1,4-dioxane (dioxane) from water using 80-microm carboxen-polydimethylsiloxane solid-phase microextraction fibers followed by either gas chromatography (GC)-flame ionization detection (FID) or GC-mass spectrometry (MS). With GC-FID, the lower limit of detection (LOD) for 1,4-dioxane is 2.5 microg/L (ppb) with a linear range of 5 to ...

A simple, rapid, and reliable method was developed for the quantitative determination of diethylene glycol (DEG) in pharmaceutical products using capillary gas chromatography with flame ionization detection. The method uses ethylene glycol as internal standard and allows for the separation of propylene glycol and DEG. The assay was linear in a DEG concentration range between 1.0 and 10.00 mg/mL...

In this work, biphenyl and biphenyl oxide were extracted by direct single drop microextraction (direct-SDME) and analyzed by gas chromatography flame ionization detection. The extraction occurred by suspending a 7 μL drop of toluene (as extracting solvent) containing acetonaphton (as internal standard) from the tip of a microsyringe in direct-SDME, respectively. The effect of different paramete...

The migration of epoxidized soy bean oil (ESBO) from the gasket in the lids of glass jars into foods, particularly those rich in edible oil, often far exceeds the legal limit (60 mg/kg). ESBO was determined through a methyl ester isomer of diepoxy linoleic acid. Transesterification occurred directly in the homogenized food. From the extracted methyl esters, the diepoxy components were isolated ...

This is a sensitive method, suitable for measuring subanogram amounts of cholesterol. Cholesterol and the internal standard, epicoprostanol (5-beta-cholestan-3-alpha-ol), are derivatized with pentafluorobenzoyl chloride and detected by electron-capture gas chromatography. The pentafluorobenzoyl esters of cholesterol and the internal standard are easily formed and possess excellent chromatograph...