Abstract Teprenone is a therapeutic anti-ulcer agent developed in Japan. As described the Japanese Pharmacopoeia (JP) 17th Edition, gas chromatography/hydrogen flame ionization detection (GC/FID) and high-performance liquid chromatography/ultraviolet (HPLC/UV) have been used for assay of active pharmaceutical ingredients (APIs) teprenone capsules, respectively. The critical aspect separation st...

The leaves of four cultivated Eucalyptus species, Eucalyptus microtheca var. Microtheca F. Muell., Eucalyptus spathulata, Eucalyptus largiflorens and Eucalyptus torquata were collected in spring from Kashan and Isfahan provinces (central region of Iran). After drying the plant materials in shade, their essential oils were obtained by hydro-distillation. The oils were analyzed by capillary gas c...

In this paper, a Least Mean Square (LMS) programming scheme is used to set the offset voltage of two operational amplifiers that were built using floating-gate transistors, enabling a 0.95 VRMS trimmer-less flame detection sensor. The programming scheme is capable of setting the offset voltage over a wide range of values by means of electron injection. The flame detection sensor consists of two...

a colorimetric method for detection and assay of mustard gas in urine after addition of thymolphthalein is reported. the detection limit was 80 ng/ml of llrine. mustard gas could also be detected in urine after extraction with gas chromatography using fid detector. the detection limit was 10 ng/ml. in addition, thiodiglycol, a metabolite of mustard gas, could be converted to mustard with concen...

The objective was to develop a simple routine method for quantitative measurement of endogenous formic acid in plasma and whole blood using headspace gas chromatography-flame ionization detection. (GC-FID). Two-hundred microliters of sample was placed in a 1-mL glass vial. Fifty microliters of aqueous ethanol (10%) was added as an internal standard and a derivatizing agent. Ethylformate formati...

in this study, both the presence and concentration of some unsaturated compounds in hexane extracts of different parts of anthemis talyschensis showing absorption at wavelength 280-450 nm were surveyed, with the view of possibly using extracts of this plant in new formulations of sunscreen creams. the hexane extracts of flower, leaf and stem of a. talyschensis , collected from northwest iran, w...

in the present study, tenorite (cuo) nanoparticles have been assayed for their catalytic properties. the decontamination reaction of chloro ethyl ethyl sulfide (cees) as an surrogate of sulfur mustard simulant have been accomplished on the surface of cuo nps with different weight ratios at ambient temperature and monitored by gas chromatography equipped with flame ionization detector (gc-fid) a...

A. Introduction B. Optical and Spectrophotometric Detectors 1. Differential refractometry 2. Ultraviolet spectrophotometry 3. Fluorescence detection 4. Infrared spectrophotometric detectors 5. Spectrophotometric detection with post-column chemical reaction C. Some Miscellaneous Detection Systems 1. The mass spectrometer as an HPLC detector 2. Radioactivity detectors 3. Density, electrochemical ...