A novel method which is based on the hydrothermal reaction was employed to synthesize LiV3O8. First, the mixture solution of LiOH, V2O5, and NH4OH was subjected to the hydrothermal reaction. The hydrothermal treatment yielded a clear, homogeneous solution. The evaporation of this solution led to the formation of a precursor gel. The gel was then heated at different temperatures in the range of ...

Starting from Ni-Co-Mn carbonate nanoparticles prepared by microreaction technology, uniform spherical particles of Ni1/3Co1/3Mn1/3CO3 with a size of 3–4 μm were obtained by a controllable hydrothermal conversion with the addition of (NH4)2CO3. Based on characterizations on the evolution of morphology and composition with hydrothermal treatment time, we clarified the mechanism of this novel met...

Nano sulfated titania was tested as solid acid heterogeneous catalyst for the synthesis of 4-(Trifluoromethyl) coumarin and coumarin derivatives under solvent-free condition. Factorial design evidenced a positive effect of reaction temperature, amount of catalyst, and solvents.  This nano-sized sulfated titania has been prepared by a sol-gel hydrothermal process. The prepared sulfated titania s...

Controllable synthesis of various ZnO nanocrystals was achieved via a simple and cost-effective hydrothermal process. The morphology evolution of the ZnO nanostructures was well monitored by tuning hydrothermal growth parameters, such as solution concentration, reaction temperature, and surfactant. As-obtained ZnO nanocrystals with different morphologies, e.g., ZnO nanorods, nanotetrapods, nano...

Rod-like hydroxyapatite nanoparticles (n-HAp) with a highly ordered nanostructure were prepared by hydrothermal synthesis from calcium chloride, and phosphoric acid, as calcium and phosphorus sources, respectively. Various surfactant families such as cationic (CTAB), anionic (SDS) and nonionic (Triton X-100) were used as regulators of the nucleation and crystal growth. The synthesized nanopowde...

The hydrothermal syntheses of hydroxyapatite and polymer composite materials were studied. The apatite precursor slurry was prepared by agitating a mixture of CaCO3 and CaHPO4·2H2O, and 3 kinds of polymeric fibers were added. The mixture was treated under hydrothermal conditions at 180 °C for 5 hours. The XRD patterns of the products showed that the products were well-crystallized hydroxyapatit...

Zinc oxide (ZnO) powders were synthesized by a simple hydrothermal process in the temperature range of 50 to 100 C. Nanocrystallites were formed by a simple hydrothermal route from aqueous solutions of zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and NaOH under controlled process conditions such as precursor concentration (0.07 to 1 mol/L), reaction pH (7 to 11) and temperatures. Single phase ZnO p...

Nano sulfated titania was tested as solid acid heterogeneous catalyst for the synthesis of 4-(Trifluoromethyl) coumarin and coumarin derivatives under solvent-free condition. Factorial design evidenced a positive effect of reaction temperature, amount of catalyst, and solvents.  This nano-sized sulfated titania has been prepared by a sol-gel hydrothermal process. The prepared sulfated titania s...

Waste problem is becoming a future problem all over the world. Magnesium wastes which can be used in recycling processes are produced by many industrial activities. Magnesium borates which have useful properties such as; high heat resistance, corrosion resistance, supermechanical strength, superinsulation, light weight, high coefficient of elasticity and so on. Addition, magnesium borates have ...

The hydrothermal method provides an effective reaction environment for the synthesis of nanocrystalline materials with high purity and well-controlled crystallinity. In this work, we started with various sizes of commercial TiO 2 powders and used the hydrothermal method to prepare TiO 2 thin films. We found that the synthesized TiO 2 nanorods were thin and long when smaller TiO 2 particleswere ...