A rapid, wafer-level, dry process for in-situ synthesis, deposition of stable nanostructured, porous metal-oxide films for gas sensors is presented. Lace-like, nanostructured films of pure SnO2 featuring high porosity (98%) are selfassembled on a target substrate by flame spray pyrolysis (FSP). The nanoparticles are mainly polyhedral and monocrystalline with a grain size of 8.7 nm and crystal s...

Traditional nanostructured design of cerium oxide catalysts typically focuses on their shape, size, and elemental composition. We report a different approach to enhance the catalytic activity of cerium oxide nanostructures through engineering high density of oxygen vacancy defects in these catalysts without dopants. The defect engineering was accomplished by a low pressure thermal activation pr...

Cluster-assembled nanostructured carbon with a fractal morphology is employed as a large-area surface scaffold for metal decoration. By depositing silver by pulsed laser ablation densely packed, distributions of metal nanoparticles are produced. The authors show, using the surface-enhanced Raman effect and the modification of fluorescence quantum yields near metallic surfaces, that silver-coate...

The sonochemical decomposition of volatile organometallic compounds produces high surface area solids that consist of agglomerates of nanometer clusters. For iron pentacarbonyl and tricarbonylnitrosylcobalt, nanostructured metals and alloys are formed; for molybdenum hexacarbonyl, the metal carbide is produced. These sonochemically produced nanostructured solids are active heterogeneous catalys...

In recent years, the field of metal-based drugs has been dominated by other existing precious metal drugs, and many researchers have focused their attention on the synthesis of various ruthenium (Ru) complexes due to their potential medical and pharmaceutical applications. The beneficial properties of Ru, which make it a highly promising therapeutic agent, include its variable oxidation states,...

We use metal-assisted chemical etching (MCE) method to fabricate nanostructured black silicon on the surface of C-Si. The Si-PIN photoelectronic detector based on this type of black silicon shows excellent device performance with a responsivity of 0.57 A/W at 1060 nm. Silicon nanocone arrays can be created using MCE treatment. These modified surfaces show higher light absorptance in the near-in...

We report the formation of wave-like structures and nanostructured fuzzes in the polycrystalline tungsten (W) irradiated with high-flux and low-energy helium (He) ions. From conductive atomic force microscope measurements, we have simultaneously obtained the surface topography and current emission images of the irradiated W materials. Our measurements show that He-enriched and nanostructured st...

Recent developments focusing on novel hydrogen storage media have helped to benchmark nanostructured carbon materials as one of the ongoing strategic research areas in science and technology. In particular, certain microporous carbon powders, carbon nanomaterials, and specifically carbon nanotubes stand to deliver unparalleled performance as the next generation of base materials for storing hyd...

In terms of the grain refinement mechanism induced by plastic straining, a novel surface mechanical attrition treatment (SMAT) was developed for synthesizing a nanostructured surface layer on metallic materials in order to upgrade the overall properties and performance. In this paper, the SMAT technique and the microstructure of the SMAT surface layer will be described. The grain refinement mec...

Nanostructured TiO2 films are deposited on a silicon substrate using 150-W power from the RF magnetron sputtering at working pressures of 3 to 5 Pa, with no substrate bias, and at 3 Pa with a substrate bias of -50 V. X-ray diffraction (XRD) analysis reveals that TiO2 films deposited on unbiased as well as biased substrates are all amorphous. Surface properties such as surface roughness and wett...