Selecting a proper support in the catalyst system plays an important role in hydrogen production via ethanol steam reforming. In this study, sol gel made alumina supports prepared for nickel (Ni) catalysts were calcined at different temperatures. A series of (Ni/AlS.G.) catalysts were synthesized by an impregnation procedure. The influence of varying the calcination temperature of the sol gel m...

TiO₂ sol was produced by the sol-gel method through the hydrolysis and the aging of tetrabutyl titanate and the TiO₂ film was obtained by dipping and uniform lifting of the acid-treated and ultrasound-treated clean glass slides into the TiO₂ sol followed by aging, drying, and calcination. The effect of the hydrolysis control agents to the formed sol was researched and the crystalline state, the...

Valerie Rapson Greece Olympia High School Advisor: Kenneth L. Marshall University of Rochester Laboratory for Laser Energetics Summer High School Research Program 2005 1. Abstract Sol-gel coatings are used on the OMEGA laser optics as anti-reflection (AR) coatings to maximize their transmittance. Over time, trace organic compounds in the laser bay contaminate these sol-gel coatings, reducing th...

The sol-gel process has emerged as an effective route for the fabrication of optical waveguides and guided wave devices and circuits. In particular, it is possible to incorporate active dopants like neodymium, erbium, and cesium for integrated optical active devices and circuits. In this paper, a review of recent research on active devices and circuits based on sol-gel process is made. Specific...

The plasma flow in the scrape-off layer (SOL) plays an important role for the particle control in magnetic fusion reactors. The flow is expected to expel Helium ashes and to retain impurities in the divertor region, if it is directed towards the divertor plate. It has been experimentally observed, however, that the flow direction is sometimes opposite; from the plate side to the SOL middle side...

The paper describes development of a sol-gel based immunoaffinity method for the steroid hormone levonorgestrel (LNG) and the effects of changes in the sol-gel matrix format on the activity of the entrapped antibodies (Abs) and on matrix structure. The best sol-gel format for Ab entrapment was found to be a tetramethoxysilane (TMOS) based matrix at a TMOS:water ratio of 1:8, containing 10% poly...

Grifolan is an antitumor (13)-ƒÀ-D-glucan with a ƒÀ-glucosyl substitution at C-6 of every three main chain units, and is produced by Grifola frondosa. Grifolan possesses two different solid-state conformations, N (native) and H (helix) (N. Ohno et al., Chem. Pharm. Bull., 34, 2555 (1986)), and both form a gel in an aqueous neutral media. In this study, the gel-to-sol or sol-to-gel transition of...

Active protein micropatterns and microarrays made by selective localization are popular candidates for medical diagnostics, such as biosensors, bioMEMS, and basic protein studies. In this paper, we present a simple fabrication process of thick (approximately 20 microm) protein micropatterning using capillary force lithography with bifunctional sol-gel hybrid materials. Because bifunctional sol-...

The phosphorus barrier layers at the doping procedure of silicon wafers were fabricated using a spin-coating method with a mixture of silica-sol and tetramethylammonium hydroxide, which can be formed at the rear surface prior to the front phosphorus spin-on-demand (SOD) diffusion and directly annealed simultaneously with the front phosphorus layer. The optimization of coating thickness was obta...

Transport of plasma from the edge pedestal gradient region into the scrape-off layer (SOL) forms the heat exhaust channel. The properties of this channel are critical for future tokamak devices. The SOL heat-flux width is believed to be set by a competition between classical parallel transport and turbulent cross-field transport. In previous work, [Myra J R, et al. 2011 J. Nucl. Mat. 415 S605] ...