A new route to highly active hopcalite catalysts via flame spray pyrolysis of an inverse microemulsion precursor is reported. The nitrate derived nanoparticles are around 15 nm in diameter and show excellent conversion of CO under ambient conditions, outperforming commercial reference hopcalite materials produced by co-precipitation.

The use of cobalt hydroxychloride [Co2(OH)3Cl] as an anode material for lithium ion batteries (LIBs) is investigated using spherical shape and ultrafine nanocrystals directly formed by spray pyrolysis from spray solution of cobalt chloride salt. Dot-mapping images of the resulting powders reveal a uniform distribution of Co, O, and Cl throughout the powder. The Co2(OH)3Cl powder prepared direct...

Tin doped In2S3 films were grown by the chemical spray pyrolysis (CSP) method using the pneumatic spray set-up and compressed air as a carrier gas. The spraying solution contained indium chloride (InCl3), thiourea [CS(NH2)2] and (SnCl4) at a molar ratio of S/In = 2.5. The deposition was carried out at 350 °C on glass substrates. The Sn doping level was changed with Sn/In = 0-8 % in solution. Th...

Thermal spray in general, plasma spray in particular, is a highly complex process with numerous interacting variables associated with generation of the spray stream, deposit formation dynamics, and the resultant property linkages. Compounding this variability further are both the spatial (different booths and different locations) and temporal (process start-stops, hardware degradation, operator...

In  this paper  thin  films of  tin sulfide (SnS) were deposited on  the glass substrates using spray pyrolysis method with the substrate temperatures in the range of 400–600℃, keeping the other deposition parameters constant. In  this work  the characteristic of SnS  thin  films  investigated. The XRD pattern and optical transmittance of thin films also are discussed. With the change in concen...

The evolution of zinc oxide nanostructures grown on graphene by alcohol-assisted ultrasonic spray pyrolysis was investigated. The evolution of structures is strongly depended on pyrolysis parameters, i.e., precursor molarity, precursor flow rate, precursor injection/deposition time, and substrate temperature. Field-effect scanning electron microscope analysis, energy dispersive X-ray spectrosco...

Pure and 10 wt% 80Al2O3-20TiO2 reinforced hydroxyapatite coatings were successfully deposited on Ti6Al4V substrate by plasma spray technique for bio medical applications. Post coating heat treatment was carried out to study the effect of heat treatment on improvement in micro structure and mechanical properties of coatings. Coating was characterized by SEM/EDAX and XRD analysis. Positive impact...

The quartz-crystal microbalance is a sensitive and versatile tool for measuring adsorption of a variety of compounds (e.g. small molecules, polymers, biomolecules, nanoparticles and cells) to surfaces. While the technique has traditionally been used for measuring adsorption to flat surfaces and thin ridged films, it can also be extended to study adsorption to nanoparticle surfaces when the nano...

An AlCoCrCuFeNi high-entropy alloy (HEA) coating was fabricated on a pure magnesium substrate using a two-step method, involving plasma spray processing and laser re-melting. After laser re-melting, the microporosity present in the as-sprayed coating was eliminated, and a dense surface layer was obtained. The microstructure of the laser-remelted layer exhibits an epitaxial growth of columnar de...