this study reports the simple process to synthesis of cuo/cui nanocomposite in a non-aqueous solution. in the conducted experiments cui and dimethyl sulfoxide (dmso) were used as the precursors. moreover, dmso had role of solvent and ligand simultaneously. in experiments the effects of oleic acid as the particles size modifier, temperature and concentration were investigated. crystalline struct...

Density, chemical, structural and vibrational studies of GexSb65Se35-x system with 0 ≤ x ≤ 20 produce by melt-quench technique were carried out using Archimedes method, Energy Dispersive Spectroscopy (EDS), X-ray diffraction (XRD) and Raman spectroscopy. All specimens are polycrystalline in nature as confirmed by XRD pattern. The compositional dependence of the XRD and Raman spectra suggests th...

Molecular beam epitaxy grown InAs/GaSb superlattices, containing InSb-like interfacial layers, were analyzed by a combination of x-ray diffraction XRD and structural refinement. The superlattice refinement from x rays SUPREX method determines with high accuracy the average thicknesses and d spacings of the individual InAs and GaSb layers in addition to standard structural parameters usually obt...

X-ray diffraction (XRD) analysis is a fundamental method to evaluate the carbon stacking structure in coal and carbon materials. However, the vagueness of XRD pattern of coal, which has the low crystallinity, often makes it difficult to evaluate the stacking structure quantitatively. In a previous study [1,2], we reported the standard analysis of carbon stacking structure in coal by XRD techniq...

in this research calcium fluoride nanoparticles and its different amount of cerium ion dopant (5%and 10%) were prepared. the mentioned nanoparticle were studied by fourier transform infrared spectroscopy (ftir) , x-ray diffraction (xrd), absorption and photoluminescence spectra (pl) and scanning electron microscopy (sem). the xrd patterns indicate a typical cubic fluorite structure and no other...

background: an early diagnosis of breast cancer relates directly to an accurate treatment plan and strategy. early detection of breast cancer before its development would be a significant reduction of morbidity and mortality rates. the aim of this preliminary study is to investigate the sensitivity of wide angle x-ray diffraction (waxrd) method on women hair samples of healthy and breast cancer...

Bioapatite, the main constituent of mineralized tissue in mammalian bones, is a calcium-phosphate-based mineral that is similar in structure and composition to hydroxyapatite. In this work, the crystallographic structure of bioapatite in human fetuses was investigated by synchrotron radiation x-ray diffraction (XRD) and microdiffraction ( micro -XRD) techniques. Rietveld refinement analyses of ...

The powders of Ba(Ce1-xZrx)0.90Y0.1O3-δ (BCZY) with 0.2 ≤ x ≤ 0.6 have been prepared by a modified sol-gel method. Triethylenetetramine (TETA) was employed as chelating agent. Phase formation of calcined powders at 1100C and sintered pellets at 1400C of BCZY were examined by an X-ray diffractrometer (XRD). XRD results showed the calcined powder and sintered pellet formed a single perovskite pha...

The deployment of in-situ miniature XRD instruments for planetary exploration requires small focus bright X-ray sources that are physically small, lightweight, robust, and power efficient. Existing miniature X-ray tubes are limited by inefficient thermionic electron sources. We have investigated the potential of carbon nanotube (CNT) field emitters for improving the efficiency and durability of...

Synchrotrons can be used to generate X-rays in order to probe materials at the atomic level. One approach is to use X-ray diffraction (XRD) to do this. The data from an XRD experiment consists of a sequence of digital image files which for a single scan could consist of hundreds or even thousands of digital images. Existing analysis software processes these images individually sequentially and ...