Nanocrystalline partially stabilised zirconia (PSZ) and yttria-fully stabilised zirconia (YSZ) powders were prepared by solution combustion process. Nanocrystalline nature of the powders was confirmed by XRD and TEM. Nanocomposite Ni/PSZ and Ni/YSZ films were electrodeposited from a suspension of nanoparticles in nickel sulfamate solution. The strengthening of the nanocomposite due to nanoparti...

Nanocrystalline titanium dioxide powder is characterized for phase analysis as well as particle size and its distribution by x-ray diffraction and small angle neutron scattering measurements. Analysis of the SANS data in the momentum transfer range q = 0.1 1.8 nm reveals an average particle size of 24.82 nm in good agreement with the particle size determined earlier by transmission electron mic...

X-ray diffraction (XRD), EDAX, AC susceptibility and resistivity measurements has been used as characterization methods for the Bi-2223 monophase target with the starting stoichiometry Bil.8F%,.3Sr2Ca2C~3.3 a. Pressure parameter is playing an important role in obtaining good superconducting properties for this compound. Critical currents and activation energy has been calculated from susceptibi...

A new BiCl3-loaded montmorillonite K10 catalyst has been prepared by solid dispersion method and was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and cyclic voltammetry (CV) measurements. BiCl3 loaded K10 (BiCl3-K10) has been used as solid acid catalyst for the synthesis of azine derivatives from benzophenone hydrazone and ketones/aldehydes by ...

Nanocrystalline zinc oxide (ZnO) particles coated with whey protein (WP) were synthesized in the weak basic aqueous solution condition at room temperature. The X-ray diffraction (XRD) and transmission electron microscopy (TEM) measurements confirmed the ZnO/WP nanoscaled composite structure. The average composite granules size was about 300 nm and the embedded ZnO nanoparticles were uniform and...

Using PVDF and ZrO2, polymer composites were prepared by sol gel method. Various measurements such as X-ray diffraction (XRD), Scanning electron microscopy (SEM) and Differential Scanning Calorimetry (DSC) were used to characterize the composites. Thermal and electrical properties of the composite samples were studied. The conductivity of composites was found to increase with increase in temper...

In-rich second phases were detected by transmission electron microscopy (TEM) in In 0.27 Ga 0.73 N multiple quantum well (MQW) samples that were annealed at 950°C for 40 h. X-ray diffraction (XRD) measurements showed a shift in the zero-order diffraction peak toward GaN, consistent with the formation of an In-poor phase remaining in the InGaN wells. Voids were also found by TEM in the MQWs afte...

X6Al2HT500 hydrotalcites, where X represents Mg, Fe, Cu or Zn were synthetized and investigated before and after gold deposition for toluene and CO total oxidation reactions. The samples have been characterized by specific areas, XRD measurements and Temperature Programmed Reduction. Concerning the toluene total oxidation, the best activity was obtained with Au/Cu6Al2HT500 catalyst with T50 at ...

Tribological properties of nanolamellar tungsten disulfide doped with zinc oxide nanoparticles were studied. Nanolamellar tungsten disulfide and ZnO nanoparticles produced by electrospark erosion of metal granules in an H2O2 solution were analyzed using the XRD, SEM and TEM techniques. According to the tribological measurements, ZnO nanoparticles did not significantly change the friction coeffi...

Diagnosis of primary and secondary coxarthrosis even today remains the privilege of medical experience and is based only on patient symptoms. We propose to use thermal analysis measurements as an objective method of diagnosing bone pathology and the degree of disease severity. Thermal analysis can be performed on few milligrams of bone tissue harvested by outpatient biopsy. For validation of th...